in neat (no solvent)
dropwise addn. of SnCl4 to tetra(isopropyl)tin with shaking, heating to 190-200°C for about 2 h; residue solidified overnight at room temp., recrystn. (petroleum ether, b.p. 40-60°C), drying under vac., elem. anal.;
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.4.3, page 92 - 93
Uglova, E. V.; Makhaev, V. D.; Shalabaev, S. H. B.; Reutov, O. A.
Zhurnal Organicheskoi Khimii, 1972 , vol. 8, p. 1815 - 1818
Zhurnal Organicheskoi Khimii, 1972 , vol. 8, p. 1769 - 1772
