1,4,8,11-四氮杂环十四烷合成路线 (共 60 条)
反应条件
ethanol beim Erhitzen anschliessend mit aethanol. KOH;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 56, p. 343,347
Inorg. Chem., , vol. 4, p. 1102,1107
反应条件
sodium hydroxide; sodium cyanide; nickel; nickel dichloride Yield given. Multistep reaction;
参考文献
Canadian Journal of Chemistry, , vol. 73, # 5 p. 685 - 695
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 6 p. 302 - 304
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 56, p. 343,347
Angewandte Chemie, , vol. 72, p. 580
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 55, p. 835
Recueil des Travaux Chimiques des Pays-Bas, , vol. 56, p. 345
反应条件
sodium hydroxide; formaldehyd; formic acid in water
参考文献
Murphy, Michael A; Malachowski, Mitchell R
Patent: US2005/85555 A1, 2005 ;
US 20050085555 A1
反应条件
potassium hydroxide; C14H30N2O4 in toluene 4 h; Ambient temperatureIrradiation;
参考文献
Jurczak, Janusz; Ostaszewski, Ryszard
Tetrahedron Letters, 1988 , vol. 29, # 8 p. 959 - 960
反应条件
1: With formic acid 24 h; Reflux; 2: With sodium hydroxide pH=> 12;
参考文献
Evangelio, Emi; Rath, Nigam P.; Mirica, Liviu M.
Dalton Transactions, 2012 , vol. 41, # 26 p. 8010 - 8021
反应条件
hydrogenchloride; hypophosphorous ether in water 5 h; Heatingvariation of time; Product distribution;
参考文献
Mollier, H.; Vincens, M.; Vidal, M.; Pasqualini, R.; Duet, M.
Bulletin de la Societe Chimique de France, 1991 , # 5 p. 787 - 795
反应条件
1: in tetrahydrofuran 1176000 h; Heating; 2: With sodium tetrahydroborate in ethanol Heating; Further stages.;
参考文献
Tripier; Lagrange; Espinosa; Denat; Guilard
Chemical Communications, 2001 , # 24 p. 2728 - 2729