1,4,8,11-四氮杂环十四烷合成路线 (共 60 条)
反应条件
sodium carbonate in acetonitrile 48 h; Heating;
参考文献
Dubois, Geraud; Tripier, Raphael; Brandes, Stephane; Denat, Franck; Guilard, Roger
Journal of Materials Chemistry, 2002 , vol. 12, # 8 p. 2255 - 2261
反应条件
in methanol; water T=20°C; 3 h;
参考文献
Le Baccon; Chuburu; Toupet; Handel; Soibinet; Dechamps-Olivier; Barbier; Aplincourt
New Journal of Chemistry, 2001 , vol. 25, # 9 p. 1168 - 1174
反应条件
1: 89 percent / H2O; methanol / 3 h / 20 °C 2: 100 percent / acetonitrile / 168 h / 20 °C 3: 93 percent / hydroxylamine hydrochloride; sodium ethoxide / ethanol / 4 h / Heating View Scheme
参考文献
Brandes, Stephane
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 1 p. 65 - 73
反应条件
Yield given. Multistep reaction;
参考文献
Yaouanc, Jean-Jacques; Bris, Nathalie Le; Gall, Guenaelle Le; Clement, Jean-Claude; Handel, Henri; Abbayes, Herve des
Journal of the Chemical Society, Chemical Communications, 1991 , # 4 p. 206 - 207
反应条件
sodium hydroxide in water T=20 - 80°C; pH=10 - 11; 4.25 h;
参考文献
Olatunde, Abiola O.; Dorazio, Sarina J.; Spernyak, Joseph A.; Morrow, Janet R.
Journal of the American Chemical Society, 2012 , vol. 134, # 45 p. 18503 - 18505
反应条件
triethylamine in dichloromethane T=20°C;
参考文献
Beijing Molecule Science and Technology Co., Ltd.
Patent: EP2163553 A1, 2010 ;
Location in patent: Page/Page column 19 ;
反应条件
triethylamine in dichloromethane T=0°C;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 16 p. 1094 - 1095
反应条件
triethylamine in ethanol Heating;
参考文献
Tsukube, Hiroshi; Adachi, Hayamitsu; Morosawa, Shiro
Journal of Organic Chemistry, 1991 , vol. 56, # 25 p. 7102 - 7108
参考文献
Mishra; Chatal
New Journal of Chemistry, 2001 , vol. 25, # 2 p. 336 - 339
反应条件
triethylamine in ethanol 15 h; Ambient temperature;
参考文献
Trabaud; Dessolin; Camplo; Kraus
Synthetic Communications, 1998 , vol. 28, # 2 p. 311 - 317