1,4,8,11-四氮杂环十四烷合成路线 （共 60 条）
参考文献
Wainwright, Kevin P.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 2117 - 2120
反应条件
sodium hydroxide in chloroform; water
Ambient temperature;
参考文献
Tsukube, Hiroshi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 615 - 620
反应条件
sodium hydroxide in chloroform; water
Ambient temperature;
参考文献
Tsukube, Hiroshi; Takagi, Kentaro; Higashiyama, Tatsuo; Iwachido, Tadashi; Hayama, Naomi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1033 - 1038
反应条件
hydrogenchloride; potassium hydroxide
1.) water, 20 deg C -> 80 deg C, pH=9-10, 24 h; 2.) 24 h, reflux; Yield given. Multistep reaction;
参考文献
Stetter, H.; Frank, W.; Mertens, R.
Tetrahedron, 1981 , vol. 37, p. 767 - 772
参考文献
Parker, Laurie L.; Lacy, Stephen M.; Farrugia, Louis J.; Evans, Cameron; Robins, David J.; O'Hare, C. Caroline; Hartley, John A.; Jaffar, Mohammed; Stratford, Ian J.
Journal of Medicinal Chemistry, 2004 , vol. 47, # 23 p. 5683 - 5689
反应条件
hydrogenchloride; hypophosphorous ether in water
5 h; Heatingvariation of time; Product distribution;
参考文献
Mollier, H.; Vincens, M.; Vidal, M.; Pasqualini, R.; Duet, M.
Bulletin de la Societe Chimique de France, 1991 , # 5 p. 787 - 795
反应条件
Yield given. Multistep reaction;
参考文献
Bernard; Yaouanc; Clement; Des Abbayes; Handel
Tetrahedron Letters, 1991 , vol. 32, # 5 p. 639 - 642
反应条件
triethylamine in methanol
T=20°C; 5.08333 h;
参考文献
Yang, David J.; Oh, Chang-Sok; Yu, Dong-Fang; Azhdarinia, Ali; Kohanim, Saady
Patent: US2007/248537 A1, 2007 ;
Location in patent: Page/Page column 37; sheet 21; sheet 22 ;
反应条件
triethylamine in methanol
T=20°C; 5 h;
参考文献
Lima, Luis M. P.; Delgado, Rita; Plutnar, Jan; Hermann, Petr; Kotek, Jan
European Journal of Inorganic Chemistry, 2011 , # 4 p. 527 - 538
反应条件
in chloroform
T=20°C; 15 h; Product distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Yang, Wen; Giandomenico, Christen M.; Sartori, Michael; Moore, Dennis A.
Tetrahedron Letters, 2003 , vol. 44, # 12 p. 2481 - 2483
