1,5,9,13-四硫杂环十六烷合成路线 (共 3 条)
反应条件
1: thioacetimidic acid 3-acetimidoylsulfanyl-propyl ester; compound with GENERIC INORGANIC NEUTRAL COMPONENT With sodium hydroxide; tetrabutylammomium bromide in benzene T=60 - 65°C; 1 h; 2: 1,3-dibromo-propane in benzene T=60 - 65°C; 1 h;
参考文献
Takido, Toshio; Toriyama, Masaharu; Ogura, Kazuhiro; Kamijo, Haruo; Motohashi, Shigeyasu; Seno, Manabu
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 6 p. 1295 - 1301
反应条件
ethanol; sodium ethanolate
参考文献
Meadow; Reid
Journal of the American Chemical Society, 1934 , vol. 56, p. 2177,2178
参考文献
Meadow; Reid
Journal of the American Chemical Society, 1934 , vol. 56, p. 2180