(S)-Alpha-氨基-2,3-二氢-4-甲氧基-7-硝基-D-基-1H-吲哚-1-戊酸合成路线 (共 6 条)
反应条件
trifluoroacetic acid T=20°C; 1 h;
参考文献
Papageorgiou, George; Corrie, John E. T.
Synthetic Communications, 2002 , vol. 32, # 10 p. 1571 - 1577
反应条件
1: 72 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide; DMAP / acetonitrile / 16 h / 20 °C 2: NaNO3; trifluoroacetic acid / 0.67 h / -15 °C View Scheme
参考文献
Papageorgiou, George; Corrie, John E.T
Tetrahedron, 2000 , vol. 56, # 41 p. 8197 - 8205
反应条件
1: 72 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide; DMAP / acetonitrile / 16 h / 20 °C 2: NaNO3; trifluoroacetic acid / 0.67 h / -15 °C View Scheme
参考文献
Papageorgiou, George; Corrie, John E.T
Tetrahedron, 2000 , vol. 56, # 41 p. 8197 - 8205
反应条件
sodium nitrate; trifluoroacetic acid T=-15°C; Nitration; 0.666667 h;
参考文献
Papageorgiou, George; Corrie, John E.T
Tetrahedron, 2000 , vol. 56, # 41 p. 8197 - 8205
反应条件
1: 43 percent / montmorillonite K10/Cu(NO3)2; acetic anhydride / CCl4 / 20 °C 2: 87 percent / TFA / 1 h / 20 °C View Scheme
参考文献
Papageorgiou, George; Corrie, John E. T.
Synthetic Communications, 2002 , vol. 32, # 10 p. 1571 - 1577
反应条件
1-(2-nitrophenyl)ethyl phosphate; DL-threo-1,4-dimercapto-2,3-butanediol in phosphate buffer photocleavage; pH=7.0; Photolysis; Quantum yieldProduct distribution;
参考文献
Papageorgiou, George; Corrie, John E.T
Tetrahedron, 2000 , vol. 56, # 41 p. 8197 - 8205