2-(3-氨基吡啶-2-基)乙酸乙酯合成路线 （共 6 条）
参考文献
SmithKline Beecham Corporation
Patent: US6624171 B1, 2003 ;
US 6624171 B1
反应条件
palladium 10 on activated carbon; hydrogen in ethanol T=25°C; P=2250.23 Torr; 18 h;
参考文献
Badland, Matthew; Devillers, Ingrid; Durand, Corinne; Fasquelle, Veronique; Gaudillire, Bernard; Jacobelli, Henry; Manage, Ajith C.; Pevet, Isabelle; Puaud, Jocelyne; Shorter, Anthony J.; Wrigglesworth, Roger
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5292 - 5296
反应条件
1: dimethylsulfoxide 2: aq. LiCl / dimethylsulfoxide 3: H2 / Pd/C / ethanol / 2068.59 Torr View Scheme
参考文献
Badland, Matthew; Devillers, Ingrid; Durand, Corinne; Fasquelle, Veronique; Gaudillire, Bernard; Jacobelli, Henry; Manage, Ajith C.; Pevet, Isabelle; Puaud, Jocelyne; Shorter, Anthony J.; Wrigglesworth, Roger
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5292 - 5296
反应条件
1: aq. LiCl / dimethylsulfoxide 2: H2 / Pd/C / ethanol / 2068.59 Torr View Scheme
参考文献
Wood, Edgar R.; Kuyper, Lee; Petrov, Kimberly G.; Hunter III, Robert N.; Harris, Philip A.; Lackey, Karen
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 4 p. 953 - 957
反应条件
hydrogenchloride in diethyl ether
参考文献
SmithKline Beecham Corporation
Patent: US6624171 B1, 2003 ;
US 6624171 B1
反应条件
sodium azide in AcOH
T=65°C; 16 h;
参考文献
Burgey, Christopher S.; Deng, Zhengwu J.
Patent: US2003/225131 A1, 2003 ;
Location in patent: Page 24 ;
US 20030225131 A1
