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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
对苄基三氟甲磺酸
合成路线
（共 128 条）
1071849-95-0
+
29540-83-8
对苄基三氟甲磺酸
→
反应条件
114772-53-1
2-氰基-4'-甲基联苯
反应条件
2,2'-bis(di-p-tolyl-phosphino)-1,1'-binaphthyl; copper(I) oxide; 1,10-phenanthroline; palladium (II) 2,4-pentanedionate in 1-methyl-pyrrolidin-2-one T=50 - 190°C; P=3375.34 Torr; Inert atmosphereMicrowave irradiation;
参考文献
Goossen, Lukas J.; Linder, Christophe; Rodriguez, Nuria; Lange, Paul P.
Chemistry - A European Journal, 2009 , vol. 15, # 37 p. 9336 - 9349
29540-83-8
对苄基三氟甲磺酸
+
172732-52-4
2-氰基苯硼酸 1,3-丙二醇酯
→
反应条件
114772-53-1
2-氰基-4'-甲基联苯
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium phosphate in toluene 1 h; Heating;
参考文献
Urawa, Yoshio; Naka, Hiroyuki; Miyazawa, Mamoru; Souda, Shigeru; Ogura, Katsuyuki
Journal of Organometallic Chemistry, 2002 , vol. 653, # 1-2 p. 269 - 278
29540-83-8
对苄基三氟甲磺酸
+
108-98-5
硫酚
→
反应条件
3699-01-2
4-甲基二苯硫醚
反应条件
N-ethyl-N,N-diisopropylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; tris(dibenzylideneacetone)dipalladium (0) in 1,4-dioxane 15 h; Heating;
参考文献
Organic Letters, , vol. 6, # 24 p. 4587 - 4590
29540-83-8
对苄基三氟甲磺酸
+
72665-98-6
→
反应条件
1595-09-1
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tetra-(n-butyl)ammonium iodide; bis(dibenzylideneacetone) palladium in tetrahydrofuran; 1-methyl-pyrrolidin-2-one T=60°C; 4 h;
参考文献
Piber, Michael; Jensen, Anne Eeg; Rottlaender, Mario; Knochel, Paul
Organic Letters, 1999 , vol. 1, # 9 p. 1323 - 1326
1086406-19-0
+
29540-83-8
对苄基三氟甲磺酸
→
反应条件
133909-96-3
4-甲基-[1,1-联苯]-3-甲腈
反应条件
2,2'-bis(di-p-tolyl-phosphino)-1,1'-binaphthyl; copper(I) oxide; 1,10-phenanthroline; palladium (II) bromide in 1-methyl-pyrrolidin-2-one T=50 - 190°C; Microwave irradiationInert atmosphere;
参考文献
Goossen, Lukas J.; Linder, Christophe; Rodriguez, Nuria; Lange, Paul P.
Chemistry - A European Journal, 2009 , vol. 15, # 37 p. 9336 - 9349
111-34-2
乙烯基正丁醚
+
29540-83-8
对苄基三氟甲磺酸
→
反应条件
161835-58-1
反应条件
triethylamine; palladium diacetate; 1,3-bis-(diphenylphosphino)propane in N,N-dimethyl-formamide T=80°C; 0.5 h;
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Penco, Sergio; Santi, Roberto
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1481 - 1486
111-34-2
乙烯基正丁醚
+
29540-83-8
对苄基三氟甲磺酸
→
反应条件
161835-58-1
反应条件
triethylamine; palladium diacetate; 2,9-dimethyl-1,10-phenanthroline in N,N-dimethyl-formamide T=60°C; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Cabri, Walter; Candiani, Ilaria; Bedeschi, Angelo; Santi, Roberto
Journal of Organic Chemistry, 1993 , vol. 58, # 26 p. 7421 - 7426
29540-83-8
对苄基三氟甲磺酸
+
97051-59-7
→
反应条件
16191-28-9
4-甲基-联苯-2-甲醛
反应条件
2,2'-bis(di-p-tolyl-phosphino)-1,1'-binaphthyl; copper(I) oxide; 1,10-phenanthroline; palladium (II) 2,4-pentanedionate in 1-methyl-pyrrolidin-2-one T=50 - 190°C; P=3375.34 Torr; Inert atmosphereMicrowave irradiation;
参考文献
Goossen, Lukas J.; Linder, Christophe; Rodriguez, Nuria; Lange, Paul P.
Chemistry - A European Journal, 2009 , vol. 15, # 37 p. 9336 - 9349
29540-83-8
对苄基三氟甲磺酸
+
71597-85-8
4-羟基苯硼酸
→
反应条件
26191-64-0
4-(4-甲基苯基)苯酚
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium fluoride; palladium diacetate in tetrahydrofuran; water T=20°C; Suzuki-Miyaura coupling; 2 h;
参考文献
Ishikawa, Shunpei; Manabe, Kei
Chemistry Letters, 2006 , vol. 35, # 2 p. 164 - 165
29540-83-8
对苄基三氟甲磺酸
+
269409-70-3
4-羟基苯硼酸频哪醇酯
→
反应条件
26191-64-0
4-(4-甲基苯基)苯酚
反应条件
lithium hydroxide; palladium diacetate in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling; 2 h;
参考文献
Ishikawa, Shunpei; Manabe, Kei
Chemical Communications, 2006 , # 24 p. 2589 - 2591
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