2-(4-甲基-3-环己烯-1-基)丙醛合成路线 (共 3 条)
反应条件
di-tert-butylazodicarboxylate; potassium tert-butylate; oxygen; 1-methyl-1H-imidazole; Cu(1,10-phenanthroline)Cl in o-di-fluorobenzene Heating;
参考文献
Marko, Istvan E.; Gautier, Arnaud; Dumeunier, Raphael; Doda, Kanae; Philippart, Freddi; Brown, Stephen M.; Urch, Christopher J.
Angewandte Chemie - International Edition, 2004 , vol. 43, # 12 p. 1588 - 1591
反应条件
bis-(1,2-dimethylpropyl)borane; pyridinium chlorochromate 1.) ether, 0 deg C, 2.) CH2Cl2, reflux; Yield given. Multistep reaction;
参考文献
Brown, Herbert C.; Kulkarni, Surendra U.; Rao, C. Gundu
Synthesis, 1980 , # 2 p. 151 - 153
反应条件
bis-(1,2-dimethylpropyl)borane; pyridinium chlorochromate 1.) ether, 2 h, 0 deg C; 2.) CH2Cl2, reflux, 2 h; Yield given. Multistep reaction;
参考文献
Brown, Herbert C.; Kulkarni, Surendra U.; Rao, C. Gundu; Patil, Vemanna D.
Tetrahedron, 1986 , vol. 42, # 20 p. 5515 - 5522