1-氯-4-(硝基甲基)苯合成路线 (共 13 条)
反应条件
sodium methylate; acetyl chloride in methanol; N,N-dimethyl acetamide Ambient temperature;
参考文献
Zen, Shonosuke; Harada, Kazuho; Nakamura, Hikaru; Iitaka, Yoichi
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 8 p. 2881 - 2884
反应条件
sodium methylate; acetyl chloride in N,N-dimethyl acetamide T=80 - 85°C;
参考文献
Zen, Shonosuke; Harada, Kazuho
Chemistry Letters, 1982 , p. 1711 - 1714
反应条件
1: With thiophenol; triethylamine; tin(ll) chloride in acetonitrile T=0°C; Nef reaction; 0.166667 h; Inert atmosphere; 2: With SnCl2·2H2O; ethanol; L-(+)-tartaric acid; water; sodium hydrogencarbonate; sodium hydrogensulfite T=40°C; Nef reaction; 18 h;
参考文献
Walvoord, Ryan R.; Berritt, Simon; Kozlowski, Marisa C.
Organic Letters, 2012 , vol. 14, # 16 p. 4086 - 4089