4,5-二甲氧基-2-硝基苯甲酰氯合成路线 （共 17 条）
反应条件
1: NH4OH 2: NaBH4 / CuSO4 3: Heating View Scheme
参考文献
Liu, Xing-Ping; Narla, Rama Krishna; Uckun, Fatih M.
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 3 p. 581 - 583
反应条件
1: NH4OH 2: NaBH4 / CuSO4 3: Heating 4: POCl2 / Heating View Scheme
参考文献
Liu, Xing-Ping; Narla, Rama Krishna; Uckun, Fatih M.
Bioorganic and Medicinal Chemistry Letters, 2003 , vol. 13, # 3 p. 581 - 583
反应条件
in benzene 1 h; Heating;
参考文献
Kuzmic, Petr; Pavlickova, Libuse; Soucek, Milan
Collection of Czechoslovak Chemical Communications, 1987 , vol. 52, # 7 p. 1780 - 1785
反应条件
1: 0.89 g / diethyl ether
2: H2 / 10percent Pd-C / ethanol / 4 h / Heating
3: 7 mg / NaNO2, H2SO4 / acetic acid; H2O / 4 h / 100 °C
4: DDQ / benzene / 10 h / Heating
5: piperidine / H2O / 15 h / Heating
View Scheme
参考文献
Ghosal, Shibnath; Saini, Kulwant S.; Frahm, August W.
Phytochemistry (Elsevier), 1983 , vol. 22, # 10 p. 2305 - 2310
反应条件
sodium hydride
1.) benzene, reflux, 2.) room temperature; Yield given. Multistep reaction;
参考文献
Singh, Rajeshwar; Jain, Padam C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 225 - 227
反应条件
1: 1.) NaH / 1.) benzene, reflux, 2.) room temperature
2: 1.)H2, 2.) aq. HCl / 1.) 10percent Pd/C / 1.) ethyl acetate, room temperature, atmospheric pressure, 2.) MeOH, reflux
View Scheme
参考文献
Singh, Rajeshwar; Jain, Padam C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 225 - 227
反应条件
1: NH4OH
2: NaBH4 / CuSO4
View Scheme
参考文献
Ogita, Haruhisa; Isobe, Yoshiaki; Takaku, Haruo; Sekine, Rena; Goto, Yuso; Misawa, Satoru; Hayashi, Hideya
Bioorganic and medicinal chemistry, 2002 , vol. 10, # 6 p. 1865 - 1871
