2-叔丁基-3,3-二甲基丁酰氯合成路线 （共 25 条）
反应条件
hydrogenchloride in diethylene glycol dimethyl ether; water T=55°C; Pummerer reaction; 6.5 h; Mechanism;
参考文献
European Journal of Organic Chemistry, , # 31 p. 6335 - 6342
反应条件
1: 65 percent / Na / NH3 / 14 h 2: 69 percent / BF3-etherate / diethyl ether 3: 70 percent / LiAlH4 / tetrahydrofuran / 18 h / Heating View Scheme
参考文献
Dubois, Jacques-Emile; Zhang, Ben Li; Lion, Claude
Tetrahedron, 1981 , vol. 37, # 24 p. 4189 - 4194
反应条件
AlCl3, aluminium chloride; dimethyl sulfoxide T=55°C; 7 h; Mechanism;
参考文献
Knorr, Rudolf
European Journal of Organic Chemistry, 2011 , # 31 p. 6335 - 6342
反应条件
1: P2S5 2: PhMgBr / tetrahydrofuran View Scheme
参考文献
Schaumann,E.; Walter,W.
Chemische Berichte, 1974 , vol. 107, p. 3562 - 3573
反应条件
tetraphosphorus decasulfide in pyridine T=140°C; 21.5 h;
参考文献
Schaumann, Ernst
Chemische Berichte, 1982 , vol. 115, p. 2755 - 2765
反应条件
pyridine; tetraphosphorus decasulfide
参考文献
Schaumann,E.; Walter,W.
Chemische Berichte, 1974 , vol. 107, p. 3562 - 3573
反应条件
1: P2S5, Py 2: monoperphthalic acid / diethyl ether View Scheme
参考文献
Elam,E.U. et al.
Journal of Organic Chemistry, 1968 , vol. 33, p. 2738 - 2741
反应条件
triethylamine in diethyl ether
1 h; Ambient temperatureultrasound sonication;
参考文献
Olah, George A.; Wu, An-hsiang; Farooq, Omar
Synthesis, 1989 , # 7 p. 566 - 567
反应条件
tri-phenylphosphine sulphide in pyridine
30 h; Heating; Product distribution;
参考文献
Schaumann, Ernst
Chemische Berichte, 1982 , vol. 115, p. 2755 - 2765
反应条件
ammonia; sodium amide in diethyl ether
参考文献
Newman,M.S. et al.
Journal of the American Chemical Society, 1960 , vol. 82, p. 2498 - 2501
