2,4,6-三甲基苯基异氰酸酯合成路线 (共 32 条)
反应条件
in benzene Substitution; Heating;
参考文献
Vovk; Kraitor; Mel'nichenko
Chemistry of Heterocyclic Compounds, 1998 , vol. 34, # 9 p. 1096 - 1097
反应条件
[VCl3(tetrahydrofuran)3]; (Bu4N)lt;PdCl3(CO)gt; in various solvent(s) T=120°C; 0.5 h; further catalysts, other reaction times; Product distribution;
参考文献
Tietz, Helmuth; Unverferth, Klaus; Schwetlick, Klaus
Zeitschrift fuer Chemie (Stuttgart, Germany), 1980 , vol. 20, # 8 p. 295 - 296
反应条件
triethylamine; α-toluene-sulfonyl chloride in diethyl ether
参考文献
Canadian Journal of Chemistry, , vol. 44, p. 297 - 305
反应条件
in benzene Substitution; Heating;
参考文献
Vovk; Kraitor; Mel'nichenko
Chemistry of Heterocyclic Compounds, 1998 , vol. 34, # 9 p. 1096 - 1097
参考文献
Habib, Nargues S.; Rieker, Anton
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1984 , vol. 39, # 11 p. 1593 - 1597
反应条件
in ethyl acetate 1.) 40 - 50 deg C, 1 h, 2.) 80 deg C, 2 h;
参考文献
Journal of Organic Chemistry, , vol. 59, # 6 p. 1465 - 1474
反应条件
in benzene Substitution; Heating;
参考文献
Vovk; Kraitor; Mel'nichenko
Chemistry of Heterocyclic Compounds, 1998 , vol. 34, # 9 p. 1096 - 1097
反应条件
bis(tetrahydrofurane)oxovanadium(IV) dichloride; (Bu4N)lt;PdCl3(CO)gt; in 1,2-dichloro-benzene T=100°C; P=750.06 Torr; cocatalyst VCl3*3THF or VOCl2*2THF, ΔH(excit), ΔS(excit), various temp., conc. and catalyst-conc.; Thermodynamic dataKinetics;
参考文献
Zeitschrift fuer Chemie (Stuttgart, Germany), , vol. 25, # 4 p. 147 - 148
参考文献
Bulletin of the Chemical Society of Japan, , vol. 51, p. 3599 - 3605
反应条件
1: benzene 2: 190 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 51, p. 3599 - 3605