3-(3-苯基-2-丙基)-2,4-戊二酮合成路线 (共 17 条)
反应条件
[Cp*Ir(SnCl3)2{SnCl2(H2O)2}] in dichloromethane T=20°C; Inert atmosphereSchlenk technique; regioselective reaction;
参考文献
Maity, Arnab Kumar; Chatterjee, Paresh Nath; Roy, Sujit
Tetrahedron, 2013 , vol. 69, # 2 p. 942 - 956
反应条件
palladium diacetate; triphenylphosphine-3,3',3''-trisulfonic acid trisodium salt in water; benzonitrile T=50°C; 24 h;
参考文献
Blart, Errol; Genet, Jean Pierre; Safi, Mohamed; Savignac, Monique; Sinou, Denis
Tetrahedron, 1994 , vol. 50, # 2 p. 505 - 514
反应条件
bismuth trifluoromethanesulphonate in nitromethane T=25°C; 4 h;
参考文献
Rueping, Magnus; Nachtsheim, Boris J.; Kuenkel, Alexander
Organic Letters, 2007 , vol. 9, # 5 p. 825 - 828
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; palladium(II) 2,4-pentanedionate; triphenylphosphine in tetrahydrofuran T=62°C; 0.5 h;
参考文献
Tetrahedron, , vol. 44, # 23 p. 7205 - 7212
反应条件
copper; Cu(II) perchlorate; ethyl acetate 8 h; Yield given;
参考文献
Journal of Organometallic Chemistry, , vol. 361, p. C57 - C60
反应条件
bismuth trifluoromethanesulphonate in nitromethane T=100°C; 2 h;
参考文献
Organic Letters, , vol. 9, # 5 p. 825 - 828
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; palladium(II) 2,4-pentanedionate; triphenylphosphine in toluene T=68°C; 5 h;
参考文献
Tetrahedron, , vol. 44, # 23 p. 7205 - 7212
反应条件
lithium chloride; bis-triphenylphosphine-palladium(II) chloride in diethylene glycol dimethyl ether T=120°C; 18 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 21 p. 2833 - 2836
反应条件
pyrrolidine; [PtCl2(η2:η2-cycloocta-1,5-diene)]; acetic acid; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=60°C; 5 h; Inert atmosphereSchlenk techniqueMicrowave irradiation; SolventTemperatureTime; regioselective reaction;
参考文献
Shibuya, Ryozo; Lin, Lu; Nakahara, Yasuhito; Mashima, Kazushi; Ohshima, Takashi
Angewandte Chemie - International Edition, 2014 , vol. 53, # 17 p. 4377 - 4381
Angew. Chem., 2014 , vol. 126, # 17 p. 4466 - 4470,5
反应条件
triethylamine; zinc(II) chloride; bis-triphenylphosphine-palladium(II) chloride in ethylene glycol dimethyl ether T=85°C; 18 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 21 p. 2833 - 2836