4-(三氟甲基)苯甲酸甲酯合成路线 (共 48 条)
反应条件
1: T=100°C; Diels-Alder cycloaddition; 16 h; 2: With potassium carbonate in acetone Heating; Further stages.;
参考文献
Volle, Jean-Noel; Schlosser, Manfred
European Journal of Organic Chemistry, 2002 , # 9 p. 1490 - 1492
反应条件
sodium hypochlorite; tetrabutylammomium bromide in ethyl acetate T=20°C; 3.5 h;
参考文献
Leduc, Andrew B.; Jamison, Timothy F.
Organic Process Research and Development, 2012 , vol. 16, # 5 p. 1082 - 1089
反应条件
dichloro bis(acetonitrile) palladium(II); silver tetrafluoroborate; oxygen; sodium t-butanolate T=45°C; Cooling with ice;
参考文献
Liu, Chao; Wang, Jing; Meng, Lingkui; Deng, Yi; Li, Yao; Lei, Aiwen
Angewandte Chemie - International Edition, 2011 , vol. 50, # 22 p. 5144 - 5148
反应条件
tellurium; Bi(NO3)3·5H2O; 5 palladium on charcoal; oxygen in methanol T=60°C; P=760.051 Torr; 8 h; Catalytic behavior; TemperatureReagent/catalyst;
参考文献
Powell, Adam B.; Stahl, Shannon S.
Organic Letters, 2013 , vol. 15, # 19 p. 5072 - 5075
反应条件
copper diacetate; acetic anhydride in N,N-dimethyl-formamide; acetonitrile T=130°C; 1 h; Sealed tube;
参考文献
Jiang, Yuyu; Pan, Shulei; Zhang, Yanghui; Yu, Jingxun; Liu, Hongqiang
European Journal of Organic Chemistry, 2014 , vol. 2014, # 10 p. 2027 - 2031
反应条件
copper(l) iodide; 1,10-phenanthroline in dimethyl sulfoxide T=60°C; 16 h; Inert atmosphere;
参考文献
Knauber, Thomas; Arikan, Fatih; Roeschenthaler, Gerd-Volker; Goossen, Lukas J.
Chemistry - A European Journal, 2011 , vol. 17, # 9 p. 2689 - 2697
反应条件
Cr(CO)3; triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride T=130°C;
参考文献
Mutin, Robert; Lucas, Christine; Thivolle-Cazat, Jean; Dufaud, Veronique; Dany, Fabienne; Basset, Jean Marie
Journal of the Chemical Society, Chemical Communications, 1988 , # 13 p. 896 - 898
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 132, # 20 p. 6900 - 6901
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O; anhydrous copper acetate; potassium carbonate in N,N-dimethyl-formamide T=60°C; 12 h; Inert atmosphere26 W fluorescent light bulbs;
参考文献
Ye, Yingda; Sanford, Melanie S.
Journal of the American Chemical Society, 2012 , vol. 134, # 22 p. 9034 - 9037
反应条件
oxygen; Titanium(IV) oxide; silver sulphate in acetonitrile T=20°C; 2 h; UV-irradiation;
参考文献
Journal of Physical Organic Chemistry, , vol. 16, # 2 p. 127 - 132