5-甲基吡啶-2-羧酸甲酯合成路线 （共 13 条）
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform
T=20°C; 15 h;
参考文献
Adamczyk, Maciej; Akireddy, Srinivasa Rao; Reddy, Rajarathnam E.
Tetrahedron Asymmetry, 2001 , vol. 12, # 17 p. 2385 - 2387
反应条件
1.1: 78 percent / m-CPBA / CHCl3 / 15 h / 20 °C
2.1: Ac2O / 3 h / Heating
2.2: 51 percent / NaOMe / methanol / 0.17 h / 0 °C
3.1: 93 percent / Ag2CO3 / CHCl3 / 120 h / 20 °C
4.1: 77 percent / AIBN; NBS / CCl4 / Heating
5.1: 34 percent / hexamethylenetetramine; aq. acetic acid / 1 h / Heating
View Scheme
参考文献
Adamczyk, Maciej; Akireddy, Srinivasa Rao; Reddy, Rajarathnam E.
Tetrahedron Asymmetry, 2001 , vol. 12, # 17 p. 2385 - 2387
反应条件
1.1: 78 percent / m-CPBA / CHCl3 / 15 h / 20 °C
2.1: Ac2O / 3 h / Heating
2.2: 51 percent / NaOMe / methanol / 0.17 h / 0 °C
3.1: 93 percent / Ag2CO3 / CHCl3 / 120 h / 20 °C
4.1: 77 percent / AIBN; NBS / CCl4 / Heating
View Scheme
参考文献
Adamczyk, Maciej; Akireddy, Srinivasa Rao; Reddy, Rajarathnam E.
Tetrahedron Asymmetry, 2001 , vol. 12, # 17 p. 2385 - 2387
