反应条件
1: 84 percent / NaI / acetone / Heating 2: 1.) Zn/Cu, DMA, 2.) a) Pd(PPh3)2Cl2 / 1.) toluene, reflux, 16 h, 2.) toluene, a) 25 deg C, 5 min, b) 55 deg C 3: 89 percent / BH3*SMe2, (R)-diphenyl-2-pyrrolidino methanol oxazaborole / tetrahydrofuran / 18 h / -20 °C View Scheme
参考文献
Bauta, William E.; Booth, John; Bos, Mary E.; DeLuca, Mark; Diorazio, Louis; Donohoe, Timothy J.; Frost, Christopher; Magnus, Nicholas; Magnus, Philip; Mendoza, Jose; Pye, Philip; Tarrant, James G.; Thom, Stephen; Ujjainwalla, Feroze
Tetrahedron, 1996 , vol. 52, # 45 p. 14081 - 14102
