1,4-二苯基-1H-1,2,3-噻唑-5-胺合成路线 (共 6 条)
参考文献
Lieber et al.
Org.Synth. Coll.Vol.IV<1963>380
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Lieber et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 654,655
Analytical Chemistry, 1957 , vol. 29, p. 916
反应条件
T=133°C; Rate constant;
参考文献
Lieber et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 5962,5964
反应条件
T=184 - 185°C; Equilibrium constant;
参考文献
Lieber et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 654,655
Analytical Chemistry, 1957 , vol. 29, p. 916
参考文献
Dimroth
Chemische Berichte, 1902 , vol. 35, p. 4059
Justus Liebigs Annalen der Chemie, 1909 , vol. 364, p. 207
反应条件
1: 80 percent / I,I-diacetoxyiodobenzene / CH2Cl2 / 1 h / Ambient temperature 2: 58 percent / potassium tert-butoxide / dimethylsulfoxide / 0.5 h 3: KOH / ethanol; H2O / 0.5 h / Heating 4: conc. aq. HCl / 5.5 h / Heating View Scheme
参考文献
Smith, Peter A. S.; Friar, James Jeffrey; Resemann, Wolfgang; Watson, Andrew C.
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3351 - 3362
参考文献
Dimroth
Chemische Berichte, 1902 , vol. 35, p. 4059
Justus Liebigs Annalen der Chemie, 1909 , vol. 364, p. 207