2-(1H-吡咯-1-基)-1-乙胺合成路线 (共 17 条)
反应条件
1: pyrrole With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide in acetonitrile T=20°C; 0.5 h; 2: 1-amino-2-chloroethane hydrochloride in acetonitrile 24 h; Reflux;
参考文献
He, Yuwei; Lin, Maohui; Li, Zhongmin; Liang, Xinting; Li, Guilong; Antilla, Jon C.
Organic Letters, 2011 , vol. 13, # 17 p. 4490 - 4493
反应条件
potassium hydroxide 2 h; Heating;
参考文献
Pleus, Susanne; Schwientek, Marion
Synthetic Communications, 1997 , vol. 27, # 17 p. 2917 - 2930
反应条件
acetic acid; ethylenediamine in 1,4-dioxane
参考文献
Syntex (U.S.A.) Inc.
Patent: US5041442 A1, 1991 ;
US 5041442 A
反应条件
hydrogenchloride; acetic acid; ethylenediamine
参考文献
Journal of the American Chemical Society, , vol. 79, p. 4144
US2770628 , ;
反应条件
hydrogenchloride; acetic acid
参考文献
Journal of the American Chemical Society, , vol. 79, p. 4144
US2770628 , ;
反应条件
sodium hydroxide; Lubrizol 2404 in acetonitrile
参考文献
Journal of Organic Chemistry, , vol. 69, # 25 p. 8668 - 8675
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Journal of Organic Chemistry, , vol. 21, p. 896
反应条件
in water 1.) room temp., 2 h; 2.) reflux 2 h; Yield given;
参考文献
Synthesis, , # 11 p. 1059 - 1060
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Chemische Berichte, , vol. 85, p. 444,445