1-(甲磺酰基)-4-硝基苯合成路线 （共 34 条）
反应条件
1: ethanol / 12 h / Ambient temperature 2: m-chloroperbenzoic acid / CH2Cl2 / 1 h / 0 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 116, # 20 p. 8978 - 8984
反应条件
(CuOTf)2.C6H6; N-methyl-2-(methylamino)ethylamine in dimethyl sulfoxide T=110°C; 20 h; Title compound not separated from byproducts.;
参考文献
Organic Letters, , vol. 4, # 25 p. 4423 - 4425
反应条件
copper(I) oxide; potassium tert-butylate; oxygen; acetylacetone T=100°C; 20 h;
参考文献
Yuan, Gaoqing; Zheng, Junhua; Gao, Xiaofang; Li, Xianwei; Huang, Liangbin; Chen, Huoji; Jiang, Huanfeng
Chemical Communications, 2012 , vol. 48, # 60 p. 7513 - 7515
反应条件
phthalic anhydride; urea hydrogen peroxide in methanol 24 h; Ambient temperature;
参考文献
Compton, Richard G.; Dryfe, Robert A. W.; Eklund, John C.; Page, Stephen D.; Hirst, Judy; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 8 p. 1673 - 1678
反应条件
titanium(IV) isopropylate; dihydrogen peroxide in dichloromethane; water T=0°C; 10 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 361-362, p. 36 - 44
反应条件
iodosylbenzene; (8S,8'S,1''S,2''S)-(salen)manganese(III) in acetonitrile -20 deg C, 1 h then to room temp.; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 50, # 32 p. 9609 - 9618
反应条件
nitronium hexafluorophosphate in nitromethane 0.166667 h; Ambient temperaturerel. rates of the nitration; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 45, # 24 p. 4973 - 4976
反应条件
sodium hydroxide in water 19 h; Heating;
参考文献
Courtin, Alfred
Helvetica Chimica Acta, 1983 , vol. 66, # 4 p. 1046 - 1052
反应条件
1: 69.7 percent / Na2SO3, 30percent NaOH / H2O / 2 h / 80 °C 2: 27.9 percent / NaOH / H2O / 19 h / Heating View Scheme
参考文献
Helvetica Chimica Acta, , vol. 66, # 4 p. 1046 - 1052
反应条件
nitrogen(IV) oxide; ozone in dichloromethane T=-10°C; Kyodai-nitration; 3 h; Product distribution; Further Variations:ReagentsSolventsTemperaturestime;
参考文献
Synthesis, , # 8 p. 1065 - 1071
