3-(2-吡啶基)-2-丙炔-1-醇合成路线 （共 7 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine T=20°C; Sonogashira reaction; Inert atmosphere;
参考文献
Chernyak, Dmitri; Gadamsetty, Surendra Babu; Gevorgyan, Vladimir
Organic Letters, 2008 , vol. 10, # 11 p. 2307 - 2310
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine Sonogashira coupling;
参考文献
Wessig, Pablo; Pick, Charlotte
Journal of Photochemistry and Photobiology A: Chemistry, 2011 , vol. 222, # 1 p. 263 - 265
反应条件
copper(l) iodide; potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp in N,N-dimethyl-formamide T=100°C; 20 h;
参考文献
Feuerstein, Marie; Doucet, Henri; Santelli, Maurice
Tetrahedron Letters, 2005 , vol. 46, # 10 p. 1717 - 1720
反应条件
in tetrahydrofuran -50 deg C, 30 min; -78 deg C, 30 min; 20 deg C, 30 min;
参考文献
Al-Arnaout, A.; Courtois, G.; Miginiac, L.
Journal of Organometallic Chemistry, 1987 , vol. 333, p. 139 - 154
反应条件
1: tetrahydrofuran 2: 28 percent / tetrahydrofuran / -50 deg C, 30 min; -78 deg C, 30 min; 20 deg C, 30 min View Scheme
参考文献
Al-Arnaout, A.; Courtois, G.; Miginiac, L.
Journal of Organometallic Chemistry, 1987 , vol. 333, p. 139 - 154
反应条件
[palladium(II)(bis(triphenylphosphanyl))dichloride] Sonogashira coupling; Inert atmosphere;
参考文献
Garcia, Lidia; Pla-Quintana, Anna; Roglans, Anna; Parella, Teodor
European Journal of Organic Chemistry, 2010 , # 18 p. 3407 - 3415
反应条件
hydrogen; nickel in ethanol T=20°C; P=37503 Torr; 4 h;
参考文献
Al-Arnaout, A.; Courtois, G.; Miginiac, L.
Journal of Organometallic Chemistry, 1987 , vol. 333, p. 139 - 154
