您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2977-45-9
合成路线
（共 30 条）
18698-96-9
邻碘苯乙酸
→
反应条件
2977-45-9
反应条件
1.1: BH3*SMe2 / tetrahydrofuran / 0 - 20 °C 2.1: Et3N / CH2Cl2 / 0 - 20 °C 3.1: NaI / acetone / Heating 4.1: n-BuLi; i-Pr2NH / hexane; tetrahydrofuran / 1 h / -78 °C 4.2: tetrahydrofuran; hexane / -78 - 20 °C 5.1: 69 percent Spectr. / PPh3; Et3N / Pd(OAc)2 / dimethylformamide; H2O / 24 h / 130 °C View Scheme
参考文献
Pletnev, Alexandre A.; Larock, Richard C.
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9428 - 9438
181717-12-4
→
反应条件
2977-45-9
反应条件
1.1: NaI / acetone / Heating 2.1: n-BuLi; i-Pr2NH / hexane; tetrahydrofuran / 1 h / -78 °C 2.2: tetrahydrofuran; hexane / -78 - 20 °C 3.1: 69 percent Spectr. / PPh3; Et3N / Pd(OAc)2 / dimethylformamide; H2O / 24 h / 130 °C View Scheme
参考文献
Pletnev, Alexandre A.; Larock, Richard C.
Journal of Organic Chemistry, 2002 , vol. 67, # 26 p. 9428 - 9438
74477-40-0
→
反应条件
2977-45-9
反应条件
1: Et2Zn / diethyl ether 2: 26 percent / 9,10-dicyanoanthracene; biphenyl; Cu(OAc)2 / acetonitrile / Irradiation View Scheme
参考文献
Hasegawa, Eietsu; Yamaguchi, Naoto; Muraoka, Hiroyasu; Tsuchida, Hiroyuki
Organic Letters, 2007 , vol. 9, # 15 p. 2811 - 2814
1590-08-5
2-甲基-3,4-二氢-2H-1-萘酮
→
反应条件
2977-45-9
反应条件
1.1: NaH / tetrahydrofuran; hexamethylphosphoric acid triamide 1.2: tetrahydrofuran; hexamethylphosphoric acid triamide 2.1: SmI2 / tetrahydrofuran 3.1: Et3N / CH2Cl2 4.1: 26 percent / 9,10-dicyanoanthracene; biphenyl; Cu(OAc)2 / acetonitrile / Irradiation View Scheme
参考文献
Hasegawa, Eietsu; Yamaguchi, Naoto; Muraoka, Hiroyasu; Tsuchida, Hiroyuki
Organic Letters, 2007 , vol. 9, # 15 p. 2811 - 2814
6742-26-3
1-氧代-1,2,3,4-四氢萘-2-羧酸乙酯
→
反应条件
2977-45-9
反应条件
1.1: NaH / dimethylformamide 2.1: aq. HBr 3.1: NaH / tetrahydrofuran; hexamethylphosphoric acid triamide 3.2: tetrahydrofuran; hexamethylphosphoric acid triamide 4.1: SmI2 / tetrahydrofuran 5.1: Et3N / CH2Cl2 6.1: 26 percent / 9,10-dicyanoanthracene; biphenyl; Cu(OAc)2 / acetonitrile / Irradiation View Scheme
参考文献
Hasegawa, Eietsu; Yamaguchi, Naoto; Muraoka, Hiroyasu; Tsuchida, Hiroyuki
Organic Letters, 2007 , vol. 9, # 15 p. 2811 - 2814
95448-03-6
→
反应条件
2977-45-9
反应条件
1.1: aq. HBr 2.1: NaH / tetrahydrofuran; hexamethylphosphoric acid triamide 2.2: tetrahydrofuran; hexamethylphosphoric acid triamide 3.1: SmI2 / tetrahydrofuran 4.1: Et3N / CH2Cl2 5.1: 26 percent / 9,10-dicyanoanthracene; biphenyl; Cu(OAc)2 / acetonitrile / Irradiation View Scheme
参考文献
Hasegawa, Eietsu; Yamaguchi, Naoto; Muraoka, Hiroyasu; Tsuchida, Hiroyuki
Organic Letters, 2007 , vol. 9, # 15 p. 2811 - 2814
529-34-0
1-四氢萘酮
→
反应条件
2977-45-9
反应条件
1.1: NaH 2.1: NaH / dimethylformamide 3.1: aq. HBr 4.1: NaH / tetrahydrofuran; hexamethylphosphoric acid triamide 4.2: tetrahydrofuran; hexamethylphosphoric acid triamide 5.1: SmI2 / tetrahydrofuran 6.1: Et3N / CH2Cl2 7.1: 26 percent / 9,10-dicyanoanthracene; biphenyl; Cu(OAc)2 / acetonitrile / Irradiation View Scheme
参考文献
Hasegawa, Eietsu; Yamaguchi, Naoto; Muraoka, Hiroyasu; Tsuchida, Hiroyuki
Organic Letters, 2007 , vol. 9, # 15 p. 2811 - 2814
36748-92-2
→
反应条件
2977-45-9
反应条件
aluminium trichloride; Petroleum ether
参考文献
Ramart; Hoch
Bulletin de la Societe Chimique de France, 1938 , vol. <5> 5, p. 848,860
209851-96-7
→
反应条件
2977-45-9
反应条件
1: Et3N / CH2Cl2 2: 26 percent / 9,10-dicyanoanthracene; biphenyl; Cu(OAc)2 / acetonitrile / Irradiation View Scheme
参考文献
Hasegawa, Eietsu; Yamaguchi, Naoto; Muraoka, Hiroyasu; Tsuchida, Hiroyuki
Organic Letters, 2007 , vol. 9, # 15 p. 2811 - 2814
209851-95-6
→
反应条件
2977-45-9
反应条件
1: SmI2 / tetrahydrofuran 2: Et3N / CH2Cl2 3: 26 percent / 9,10-dicyanoanthracene; biphenyl; Cu(OAc)2 / acetonitrile / Irradiation View Scheme
参考文献
Hasegawa, Eietsu; Yamaguchi, Naoto; Muraoka, Hiroyasu; Tsuchida, Hiroyuki
Organic Letters, 2007 , vol. 9, # 15 p. 2811 - 2814
首页
上一页
1
2
3
下一页
末页
到第
页
确定
