2,3,3-三甲基丁烷-2-胺合成路线 （共 7 条）
反应条件
potassium hydroxide
T=200°C; 24 h;
参考文献
Timberlake, Jack W.; Alender, Jeff; Garner, Archie W.; Hodges, Melvin L.; Oezmeral, Cenan; et al.
Journal of Organic Chemistry, 1981 , vol. 46, # 10 p. 2082 - 2089
反应条件
1: 64 percent / H2SO4 / acetic acid / 12 h / Ambient temperature
2: 86 percent / aq. KOH / 24 h / 200 °C
View Scheme
参考文献
Timberlake, Jack W.; Alender, Jeff; Garner, Archie W.; Hodges, Melvin L.; Oezmeral, Cenan; et al.
Journal of Organic Chemistry, 1981 , vol. 46, # 10 p. 2082 - 2089
反应条件
methanol; sodium hydroxide
参考文献
Stiles; Mayer
Journal of the American Chemical Society, 1959 , vol. 81, p. 1497,1503
参考文献
Vejdelek; Trcka
Experientia, 1959 , vol. 15, p. 215
反应条件
sodium hydroxide in ethylene glycol
参考文献
Prochazka,M.
Collection of Czechoslovak Chemical Communications, 1976 , vol. 41, p. 1557 - 1564
反应条件
1.1: magnesium / diethyl ether / 1 h / 20 °C / Inert atmosphere
1.2: 5 h / 20 °C
2.1: sulfuric acid; acetic acid / 12 h / 20 °C
3.1: potassium hydroxide / water / 24 h / Autoclave
View Scheme
参考文献
Liu, Xiang; Ge, Kaiqi; Guan, Pei; He, Pang; Li, Yunfei; Shi, Yanhui; Cao, Changsheng
Journal of Chemical Research, 2012 , vol. 36, # 5 p. 288 - 289
反应条件
(i) Et2O, (ii) H2O; Multistep reaction;
参考文献
Davis,F.A.; Mancinelli,P.A.
Journal of Organic Chemistry, 1977 , vol. 42, # 2 p. 398 - 399
