1-(2-甲基-2-丙基)-4-(苯基乙炔基)苯合成路线 (共 14 条)
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran; pentane T=25°C; 4 h; Inert atmosphere;
参考文献
Truong, Thanh; Daugulis, Olafs
Organic Letters, 2011 , vol. 13, # 16 p. 4172 - 4175
反应条件
1,2-bis(2-thienylethynyl)benzene; bis-triphenylphosphine-palladium(II) chloride; triethylamine in acetonitrile Sonogashira coupling; 17 h; Inert atmosphereReflux;
参考文献
Atobe, Shingo; Sonoda, Motohiro; Suzuki, Yuki; Shinohara, Hiroyuki; Yamamoto, Takuya; Ogawa, Akiya
Chemistry Letters, 2011 , vol. 40, # 9 p. 925 - 927
反应条件
1: iodobenzene; acetylenecarboxylic acid With 1-methyl-pyrrolidin-2-one; 1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride T=20°C; Sonogashira coupling; 12 h; 2: 1-bromo-4-(1,1-dimethylethyl)benzene T=90°C; 12 h;
参考文献
Moon, Jeongju; Jeong, Miso; Nam, Hyungoog; Ju, Jinhun; Moon, Joong Ho; Jung, Hyun Min; Lee, Sunwoo
Organic Letters, 2008 , vol. 10, # 5 p. 945 - 948
参考文献
Martelli,G. et al.
Journal of the Chemical Society [Section] B: Physical Organic, 1970 , p. 1413 - 1418