1-氟-3-(2-苯基乙炔)苯合成路线 (共 5 条)
反应条件
sodium tetrachloropalladium (II); sodium lauryl sulfate; sodium hydroxide in water T=20°C; Sonogashira coupling; 8 h;
参考文献
Saha, Debasree; Dey, Raju; Ranu, Brindaban C.
European Journal of Organic Chemistry, 2010 , # 31 p. 6067 - 6071
反应条件
potassium phosphate; C30H37Br2N3Pd(2-) in dimethyl sulfoxide T=100°C; Sonogashira Cross-Coupling; 1 h;
参考文献
Yang, Longguang; Li, Yunfei; Chen, Qian; Du, Yufeng; Cao, Changsheng; Shi, Yanhui; Pang, Guangsheng
Tetrahedron, 2013 , vol. 69, # 25 p. 5178 - 5184
反应条件
sodium t-butanolate in 1,4-dioxane T=20 - 125°C; 36 h; Inert atmosphere;
参考文献
Truong, Thanh; Daugulis, Olafs
Organic Letters, 2011 , vol. 13, # 16 p. 4172 - 4175
反应条件
[bbim]BF4; triethylamine; palladium dichloride T=30°C; Sonogashira reaction; 2 h; sonication;
参考文献
Gholap, Atul R.; Venkatesan; Pasricha, Renu; Daniel, Thomas; Lahoti, Rajgopal J.; Srinivasan, Kumar V.
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4869 - 4872
参考文献
Martelli,G. et al.
Journal of the Chemical Society [Section] B: Physical Organic, 1970 , p. 1413 - 1418