N-叔戊基-1,1-二甲基炔丙基胺合成路线 (共 5 条)
反应条件
water; copper; copper(l) chloride T=25 - 35°C; Alkylation; 2 h;
参考文献
Sosnovsky, George; Jawdosiuk, Mikolaj; Clumpner, J. Michael
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2000 , vol. 55, # 1 p. 109 - 126
反应条件
1: liq. NH3, KOH 2: H2 / Raney-Ni / ethanol 3: Cu, aq. KOH View Scheme
参考文献
Hennion,G.F.; DiGiovanna,C.V.
Journal of Organic Chemistry, 1965 , vol. 30, p. 2645 - 2650
反应条件
1: H2 / Raney-Ni / ethanol 2: Cu, aq. KOH View Scheme
参考文献
Hennion,G.F.; DiGiovanna,C.V.
Journal of Organic Chemistry, 1965 , vol. 30, p. 2645 - 2650
反应条件
hydrogen; Lindlar's catalyst in various solvent(s) T=-10°C; Catalytic hydrogenation; P=2585.74 Torr;
参考文献
Sosnovsky, George; Jawdosiuk, Mikolaj; Clumpner, J. Michael
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2000 , vol. 55, # 1 p. 109 - 126
反应条件
hydrogen; palladium on activated charcoal in various solvent(s) Catalytic hydrogenation; P=2120.31 - 2947.74 Torr;
参考文献
Sosnovsky, George; Jawdosiuk, Mikolaj; Clumpner, J. Michael
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2000 , vol. 55, # 1 p. 109 - 126