O,O′-二乙基二硫代磷酸酯合成路线 （共 159 条）
反应条件
Ambient temperaturesealed amp.; Product distributionMechanism;
参考文献
Zimin, M. G.; Kamalov, R. M.; Cherkasov, R. A.; Pudovik, A. N.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 371 - 378
反应条件
Ambient temperaturesealed amp.; Product distributionMechanism;
参考文献
Zimin, M. G.; Kamalov, R. M.; Cherkasov, R. A.; Pudovik, A. N.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 371 - 378
参考文献
Perregaard,J. et al.
Bulletin des Societes Chimiques Belges, 1977 , vol. 86, p. 321 - 328
反应条件
Ambient temperaturesealed amp.; Product distributionMechanism;
参考文献
Zimin, M. G.; Kamalov, R. M.; Cherkasov, R. A.; Pudovik, A. N.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 371 - 378
反应条件
in 1,4-dioxane
T=40 - 45°C; ratio; Product distribution;
参考文献
Nasakin, O. E.; Nikolaev, E. G.; Terent'ev, P. B.; Bulai, A. Kh.; Khaskin, B. A.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 3 p. 577 - 583,510 - 516
反应条件
3,3',5,5'-tetra-tert-butyl-4,4'-diphenoquinone in toluene
T=45°C; 6 h;
参考文献
Liakumovich, A. G.; Kadyrova, V. Kh.; Mukmeneva, N. A.; Bukharov, S. V.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 1.2 p. 260 - 261,237
反应条件
hydrogenchloride in chloroform
T=-5°C; 1 h;
参考文献
Sapozhnikova, Zh.Z.; Prokof'eva, A.F.; Volkova, V.N.; Mel'nikov, N.N.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 11.1 p. 2451 - 2460,2275 - 2284
参考文献
Almasi,L.; Paskucz,L.
Chemische Berichte, 1965 , vol. 98, p. 3546 - 3553
Full Text Show Details
Woo, Edward J.; Kalbacher, Barbara J.; McEwen, William E.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 269 - 278
反应条件
in chloroform-d1
byproducts: acetic acid; To the Mo-compd. in CDCl3 is added (EtO)2PS2H, causing rapid darkening.; Pptn. of colorless crystals; (31)P-NMR and (1)H-NMR spectroscopy;
参考文献
Noble, Mark E.
Inorganic Chemistry, 1990 , vol. 29, p. 1337 - 1342
反应条件
in 1,4-dioxane
T=40 - 45°C; ratio; Product distribution;
参考文献
Nasakin, O. E.; Nikolaev, E. G.; Terent'ev, P. B.; Bulai, A. Kh.; Khaskin, B. A.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 3 p. 577 - 583,510 - 516
