O,O′-二乙基二硫代磷酸酯合成路线 （共 159 条）
反应条件
P=15 Torr; 8 h; Further byproducts given;
参考文献
Ofitserov, E. N.; Sinyashin, O. G.; Batyeva, E. S.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 4 p. 738 - 745,602 - 608
反应条件
T=60 - 65°C; 7 h; Heating;
参考文献
Ofitserov, E. N.; Sinyashin, O. G.; Batyeva, E. S.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 4 p. 738 - 745,602 - 608
反应条件
dicyclohexyl-carbodiimide in acetonitrile
Ambient temperature;
参考文献
Mikolajczyk, Marian; Kielbasinski, Piotr; Basinski, Wlodzimierz
Journal of Organic Chemistry, 1984 , vol. 49, # 5 p. 899 - 908
反应条件
in benzene
T=78°C; 2 h;
参考文献
Zaslona, Alexander T.; Hall, C. Dennis
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3059 - 3064
反应条件
thiamine diphosphate; diethylazodicarboxylate in benzene
T=50°C; 6 h;
参考文献
Mlotkowska, B.
Journal fuer Praktische Chemie (Leipzig), 1989 , vol. 331, # 3 p. 380 - 386
反应条件
triethylamine; benzene
参考文献
Meinhardt; Vogel
Journal of Organic Chemistry, 1959 , vol. 24, p. 1604
参考文献
Norman et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 161
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Lubrizol Corp.
Patent: US2802856 , 1953 ;
反应条件
T=60 - 65°C; 7 h; Heating;
参考文献
Ofitserov, E. N.; Sinyashin, O. G.; Batyeva, E. S.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 4 p. 738 - 745,602 - 608
反应条件
4 A molecular sieve in diethyl ether
1 h; Ambient temperature;
参考文献
Aleshnikova, T. V.; Prokof'eva, A. F.; Manaev, S. A.; Negrebetskii, V. V.; Grapov, A. F.; Mel'nikov, N. N.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 4 p. 800 - 806,708 - 713
反应条件
in diethyl ether
Ambient temperatureother solvents; MechanismProduct distribution;
参考文献
Mikolajczyk, Marian; Kielbasinski, Piotr; Basinski, Wlodzimierz
Journal of Organic Chemistry, 1984 , vol. 49, # 5 p. 899 - 908
