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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
碳酸氢钾
合成路线
（共 130 条）
108-73-6
间苯三酚
+
298-14-6
碳酸氢钾
→
反应条件
83-30-7
2,4,6-三羟基苯甲酸
反应条件
2,3-dihydroxybenzoate decarboxylase from Aspergillus oryzae in aq. phosphate buffer T=30°C; Kolbe-Schmidt Synthesis; 24 h; Enzymatic reaction; regioselective reaction;
参考文献
Wuensch, Christiane; Gross, Johannes; Steinkellner, Georg; Lyskowski, Andrzej; Gruber, Karl; Glueck, Silvia M.; Faber, Kurt
RSC Advances, 2014 , vol. 4, # 19 p. 9673 - 9679
39651-54-2
+
298-14-6
碳酸氢钾
→
反应条件
100-15-2
N-甲基对硝基苯胺
反应条件
2,3,11,12-dicyclohexano-1,4,7,10,13,16-hexaoxacyclo-octadecane in N,N-dimethyl-formamide T=30°C; var. solvents, isotope effect; Rate constant;
参考文献
Shinkai, Seiji; Nakashima, Naotoshi; Kunitake, Toyoki
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 840 - 845
78466-25-8
+
298-14-6
碳酸氢钾
→
反应条件
100-15-2
N-甲基对硝基苯胺
反应条件
2,3,11,12-dicyclohexano-1,4,7,10,13,16-hexaoxacyclo-octadecane in N,N-dimethyl-formamide T=30°C; var. solvents; Rate constant;
参考文献
Shinkai, Seiji; Nakashima, Naotoshi; Kunitake, Toyoki
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 3 p. 840 - 845
90-15-3
1-萘酚
+
298-14-6
碳酸氢钾
→
反应条件
86-48-6
1-羟基-2-萘甲酸
反应条件
salicylic acid decarboxylase from Trichosporon moniliiforme in aq. phosphate buffer T=30°C; Kolbe-Schmidt Synthesis; 24 h; Enzymatic reaction; regioselective reaction;
参考文献
Wuensch, Christiane; Gross, Johannes; Steinkellner, Georg; Lyskowski, Andrzej; Gruber, Karl; Glueck, Silvia M.; Faber, Kurt
RSC Advances, 2014 , vol. 4, # 19 p. 9673 - 9679
123-30-8
对氨基苯酚
+
298-14-6
碳酸氢钾
→
反应条件
89-57-6
美沙啦嗪(5-氨基水杨酸)
反应条件
2,3-dihydroxybenzoate decarboxylase from Aspergillus oryzae in aq. phosphate buffer T=30°C; Kolbe-Schmidt Synthesis; 24 h; Enzymatic reaction; regioselective reaction;
参考文献
Wuensch, Christiane; Gross, Johannes; Steinkellner, Georg; Lyskowski, Andrzej; Gruber, Karl; Glueck, Silvia M.; Faber, Kurt
RSC Advances, 2014 , vol. 4, # 19 p. 9673 - 9679
298-14-6
碳酸氢钾
+
108-46-3
间苯二酚
→
反应条件
303-07-1
2,6-二羟基苯甲酸
反应条件
2,6-dihydroxybenzoatedecarboxylase fromRhizobium sp in aq. phosphate buffer T=30°C; Kolbe-Schmidt Synthesis; 24 h; Enzymatic reaction; regioselective reaction;
参考文献
Wuensch, Christiane; Gross, Johannes; Steinkellner, Georg; Lyskowski, Andrzej; Gruber, Karl; Glueck, Silvia M.; Faber, Kurt
RSC Advances, 2014 , vol. 4, # 19 p. 9673 - 9679
298-14-6
碳酸氢钾
+
108-46-3
间苯二酚
→
反应条件
89-86-1
2,4-二羟基苯甲酸
+
303-07-1
2,6-二羟基苯甲酸
反应条件
Trichosporon moniliiforme WU-0401 salicylic acid decarboxylase T=30°C; enzymatic Kolbe-Schmitt reaction; pH=7; 1 h; aq. phosphate bufferEnzymatic reaction; regioselective reaction;
参考文献
Kirimura, Kohtaro; Gunji, Hiroaki; Wakayama, Rumiko; Hattori, Takasumi; Ishii, Yoshitaka
Biochemical and Biophysical Research Communications, 2010 , vol. 394, # 2 p. 279 - 284
106-41-2
4-溴苯酚
+
298-14-6
碳酸氢钾
→
反应条件
89-55-4
5-溴水杨酸
反应条件
2,3-dihydroxybenzoate decarboxylase from Aspergillus oryzae in aq. phosphate buffer T=30°C; Kolbe-Schmidt Synthesis; 24 h; Enzymatic reaction; regioselective reaction;
参考文献
Wuensch, Christiane; Gross, Johannes; Steinkellner, Georg; Lyskowski, Andrzej; Gruber, Karl; Glueck, Silvia M.; Faber, Kurt
RSC Advances, 2014 , vol. 4, # 19 p. 9673 - 9679
298-14-6
碳酸氢钾
+
108-46-3
间苯二酚
→
反应条件
89-86-1
2,4-二羟基苯甲酸
反应条件
in water T=160°C; Kolbe-Schmidt Synthesis; P=30003 Torr; 0.0902778 h; TemperatureTimePressure;
参考文献
Hessel, Volker; Hofmann; Loeb; Loehndorf; Loewe; Ziogas
Organic Process Research and Development, 2005 , vol. 9, # 4 p. 479 - 489
298-14-6
碳酸氢钾
+
108-46-3
间苯二酚
→
反应条件
89-86-1
2,4-二羟基苯甲酸
+
303-07-1
2,6-二羟基苯甲酸
反应条件
Trichosporon moniliiforme WU-0401 salicylic acid decarboxylase T=30°C; enzymatic Kolbe-Schmitt reaction; pH=7; 1 h; aq. phosphate bufferEnzymatic reaction; regioselective reaction;
参考文献
Kirimura, Kohtaro; Gunji, Hiroaki; Wakayama, Rumiko; Hattori, Takasumi; Ishii, Yoshitaka
Biochemical and Biophysical Research Communications, 2010 , vol. 394, # 2 p. 279 - 284
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