n-辛基-β-D-吡喃葡萄糖苷合成路线 (共 30 条)
反应条件
sodium methylate in methanol T=20°C; Zemplen reaction; 3 h;
参考文献
Ferlin, Nadege; Grassi, Diego; Ojeda, Carlos; Castro, Mariano J.L.; Grand, Eric; Fernandez Cirelli, Alicia; Kovensky, Jose
Carbohydrate Research, 2008 , vol. 343, # 5 p. 839 - 847
反应条件
palladium on activated charcoal; hydrogen T=20°C; 13 h; Overall yield = 90 percent;
参考文献
Chemistry Letters, , vol. 42, # 10 p. 1235 - 1237
反应条件
sulfuric acid in 1,4-dioxane Yields of byproduct given;
参考文献
Adasch, Volker; Hoffmann, Bettina; Milius, Wolfgang; Platz, Gerhard; Voss, Gundula
Carbohydrate Research, 1998 , vol. 314, # 3-4 p. 177 - 187
反应条件
phosphate buffer; lactase from Kluyveromyces lactis in nitrobenzene T=50°C; 1 h;
参考文献
Mitsuo, Naoki; Takeichi, Hiroshi; Satoh, Toshio
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 3 p. 1183 - 1187
反应条件
hydrogen; palladium on activated charcoal T=20°C;
参考文献
Tetrahedron, , vol. 59, # 45 p. 8869 - 8875
反应条件
1: 66 percent / p-TsOH / CH2Cl2 / 15 h / 20 °C 2: H2 / Pd/C / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 59, # 45 p. 8869 - 8875
反应条件
immobilized β-glucosidase G 0395 from almonds (EC 3.2.1.21) in water T=20°C; 144 h;
参考文献
Balogh, Terez; Boross, Laszlo; Kosary, Judit
Tetrahedron, 2004 , vol. 60, # 3 p. 679 - 682
反应条件
almond β-glucosidase in acetate buffer; acetonitrile T=50°C; pH=4.4; 72 h;
参考文献
Jerkovic, Igor; Mastelic, Josip
Croatica Chemica Acta, 2004 , vol. 77, # 3 p. 529 - 535
反应条件
1: 9.1 g / lithium carbonate / CH2Cl2 / 18 h / 30 °C 2: 67 percent / sodium methoxide / methanol / 24 h / 20 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 45, # 2 p. 461 - 465
反应条件
C2HF6NO4S2*CH2N4 in water T=80°C; 24 h; Reagent/catalyst; Overall yield = 40 percent; stereoselective reaction;
参考文献
Carbohydrate Research, , vol. 381, p. 12 - 18