2-乙酰氨基-2-脱氧-beta-d-吡喃葡萄糖叠氮化物合成路线 (共 18 条)
反应条件
1: hydrogen bromide / dichloromethane; acetic acid / 5 h / 0 °C 2: tetra-N-butylammonium azide / dichloromethane 3: sodium methylate / methanol / 1 h View Scheme
参考文献
Chemistry - A European Journal, , vol. 19, # 44 p. 14836 - 14851
反应条件
1: tetra-N-butylammonium azide / dichloromethane 2: sodium methylate / methanol / 1 h View Scheme
参考文献
Chemistry - A European Journal, , vol. 19, # 44 p. 14836 - 14851
反应条件
1: pyridine 2: sodium methylate; methanol View Scheme
参考文献
Chemische Berichte, , vol. 89, p. 1521,1529
反应条件
1: pyridine 2: sodium methylate; methanol View Scheme
参考文献
Chemische Berichte, , vol. 89, p. 1521,1529
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; 2 h;
参考文献
Joseph, Ryan; Dyer, Frank Brock; Garner, Philip
Organic Letters, 2013 , vol. 15, # 4 p. 732 - 735
反应条件
Campylobacter jejuni UDP-Glc/GlcNAc-4'-epimerase; human His6-propeptide-placental catβ1,4-galactosyltransferase 1 fusion protein; alkaline phosphatase Enzymatic reaction;
参考文献
Adamiak, Kathrin; Anders, Thorsten; Henze, Manja; Keul, Helmut; Moeller, Martin; Elling, Lothar
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 84, p. 108 - 114
反应条件
1: With sodium hydride in N,N-dimethyl-formamide T=0 - 20°C; 2: With barium dihydroxide; BaO in dichloromethane; N,N-dimethyl-formamide Heating;
参考文献
Thiele, Gabriela; Rottmann, Antje; Germer, Antje; Kleinpeter, Erich; Spindler, Klaus-Dieter; Synstad, Bjornar; Eijsink, Vincent G. H.; Peter, Martin G.
Journal of Carbohydrate Chemistry, 2002 , vol. 21, # 6 p. 471 - 489
反应条件
1: 76 percent / formic acid / 0.5 h / Ambient temperature
2: 82 percent / barium oxide, barium hydroxide octahydrate / dimethylformamide / 2 h / Ambient temperature; 1.) N,N-dimethylformamide, RT, 2 h, 2.) chloroform, reflux, 2 h
View Scheme
参考文献
Shaban, Mohammed Abd El-Monem; Jeanloz, Roger W.
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 11 p. 3570 - 3576