1: With N,N,N',N'-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a;2',1'-c][1,4] diazepine-2,12-diamine in N,N-dimethyl-formamide
T=20°C; 72 h; Inert atmosphereGloveboxUV-irradiation;
2: With hydrogenchloride in water
T=0°C; pH=< 3; Inert atmosphere; chemoselective reaction;
参考文献
Doni, Eswararao; Mondal, Bhaskar; O'Sullivan, Steven; Tuttle, Tell; Murphy, John A.
Journal of the American Chemical Society, 2013 , vol. 135, # 30 p. 10934 - 10937
