1: 1.) NaOEt / 1.) EtOH, 50 deg C, 1 h, 2.) EtOH, 50 deg C, 6 h 2: KOH / ethanol / 16 h View Scheme

1: 1.) NaOEt / 1.) EtOH, 50 deg C, 1 h, 2.) EtOH, 50 deg C, 6 h 2: KOH / ethanol / 16 h View Scheme

sodium hydride

暂无反应条件数据

1: 61 percent / NaH / tetrahydrofuran / Heating 2: AD-mix-β <(DHQD)2PHAL> / 2-methyl-propan-2-ol; H2O / 24 h / 0 °C 3: 87 percent / pyridine / CHCl3 / 24 h / Ambient temperature 4: 67 percent / LiBr / tetrahydrofuran / 40 h / 55 °C 5: 53 percent / Bu3SnH, AIBN / benzene / 0.33 h / Heating 6: 100 percent / 6N HCl / 6 h / Heating View Scheme