3,4-二甲氧基-5-羟基苯甲醛合成路线 （共 37 条）
反应条件
sodium carbonate in acetone 6 h; Reflux;
参考文献
Huang, Guan-Jhong; Bhaskar Reddy, M. Vijaya; Kuo, Ping-Chung; Huang, Chieh-Hung; Shih, Hung-Cheng; Lee, E.-Jian; Yang, Mei-Lin; Leu, Yann-Lii; Wu, Tian-Shung
European Journal of Medicinal Chemistry, 2012 , vol. 48, p. 371 - 378
反应条件
sodium carbonate in acetone 5 h; Reflux;
参考文献
Cervi, Aymeric; Aillard, Paul; Hazeri, Nourallah; Petit, Laurent; Chai, Christina L. L.; Willis, Anthony C.; Banwell, Martin G.
Journal of Organic Chemistry, 2013 , vol. 78, # 19 p. 9876 - 9882
反应条件
Yield given. Multistep reaction;
参考文献
Heterocycles, , vol. 20, # 12 p. 2425 - 2428
反应条件
sodium carbonate in acetone 5 h; Heating;
参考文献
Synthetic Communications, , vol. 28, # 9 p. 1517 - 1524
反应条件
1: 96 percent / 125 °C 2: 1.) butyllithium, B(OBu)3, 2.) 30percent H2O2, 3.) (NH4)2SO4 View Scheme
参考文献
Synthetic Communications, , vol. 11, # 12 p. 969 - 978
反应条件
1: 29 g / K2CO3 / acetone / 3 h / Heating 2: 1.) H2CO3H; 2.) 5 percent KOH / 1.) formic acid, overnight; 2.) ether, 2 h 3: dimethylformamide / 4 h / Heating 4: Raney-Ni / H2O; formic acid / 2 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 2 p. 660 - 667
反应条件
nickel in formic acid; water 2 h; Heating; Yield given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 2 p. 660 - 667
反应条件
1: 60 percent / NaOH, Cu / H2O / 25.5 h / 101 °C 2: 70 percent / Na2CO3 / acetone / 5 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 28, # 9 p. 1517 - 1524
反应条件
1: dimethylformamide / 4 h / Heating 2: Raney-Ni / H2O; formic acid / 2 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 2 p. 660 - 667
反应条件
hydrogenchloride in ethanol Heating;
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 447 - 451
