4-(2-噻吩基)苯甲酸合成路线 (共 13 条)
反应条件
Eosin in dimethyl sulfoxide Photolysis;
参考文献
Chemistry of Materials, , vol. 25, # 1 p. 90 - 97
反应条件
tris(dibenzylideneacetone)dipalladium (0); Sasrin resin; potassium carbonate; benzotriazol-1-ol; N'-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; trifluoroacetic acid 1) CH2Cl2, rt, 20 h; 2) DMF, rt, 20 h; 3) CH2Cl2, rt, 30 min; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 61, # 15 p. 5169 - 5171
反应条件
1: Et3N, (PhO)2P(O)N3 / dimethylformamide / 37 °C
2: toluene / Heating
View Scheme
参考文献
Axton, Christopher A.; Billingham, Michael E. J.; Bishop, Paul M.; Gallagher, Peter T.; Hicks, Terence A.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 17 p. 2203 - 2214