1-(2-氯苯基)-3-苯基脲合成路线 （共 7 条）
反应条件
1: benzoyl hydroxylamine With 4-methyl-morpholine; bromo-dimethylsulfonium bromide in 1,2-dichloro-ethane
T=0°C; Lossen rearrangement; 2 h; Inert atmosphere;
2: 2-chloro-aniline in 1,2-dichloro-ethane
T=0 - 80°C; Lossen rearrangement;
参考文献
Yadav, Deepak K.; Yadav, Arvind K.; Srivastava, Vishnu P.; Watal, Geeta; Yadav, Lal Dhar S.
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2890 - 2893
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; caesium carbonate; (9,9-dimethyl-9H-xanthene-4,5-diyl)bis(bis(3,5-bis(trifluoromethyl)phenyl)phosphine) in 1,4-dioxane
T=100°C; 1 h;
参考文献
Sergeev; Artamkina; Beletskaya
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 12 p. 1741 - 1752
反应条件
in dichloromethane
T=20°C; 3 h;
参考文献
Clayden, Jonathan; Turner, Hazel; Pickworth, Mark; Adler, Thomas
Organic Letters, 2005 , vol. 7, # 15 p. 3147 - 3150
Title/Abstract Full Text View citing articles Show Details
Adler, Thomas; Bonjoch, Josep; Clayden, Jonathan; Font-Bardia, Merce; Pickworth, Mark; Solans, Xavier; Sole, Daniel; Vallverdu, Lluis
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 17 p. 3173 - 3183
反应条件
pyridine; lead(IV) acetate in dichloromethane
Heating;
参考文献
Debroy, Abhijit; Nandy Mazumdar, Sujit; Barua, Parag D.; Mahajan, Mahinder P.
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 315 - 316
反应条件
1: ethanol / Ambient temperature
2: 65 percent / lead tetraacetate, pyridine / CH2Cl2 / Heating
View Scheme
参考文献
Debroy, Abhijit; Nandy Mazumdar, Sujit; Barua, Parag D.; Mahajan, Mahinder P.
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 315 - 316
反应条件
1: ethanol / Ambient temperature
2: 65 percent / lead tetraacetate, pyridine / CH2Cl2 / Heating
View Scheme
参考文献
Debroy, Abhijit; Nandy Mazumdar, Sujit; Barua, Parag D.; Mahajan, Mahinder P.
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 1 p. 315 - 316
参考文献
Sah
Journal of the Chinese Chemical Society (Peking), 1946 , vol. 13, p. 22,26,27
Recueil des Travaux Chimiques des Pays-Bas, 1940 , vol. 59, p. 231,233,234
