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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
29906-47-6
合成路线
（共 8 条）
29906-47-6
→
反应条件
109055-55-2
反应条件
1: 70 percent / lithium aluminium hydride / tetrahydrofuran / 72 h / Heating 2: 59 percent / formic acid / 10 h / Heating View Scheme
参考文献
Charles, Elisabeth S.; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 752 - 756
29906-47-6
→
反应条件
22317-01-7
1,3-二甲基-哌嗪
反应条件
1: 70 percent / lithium aluminium hydride / tetrahydrofuran / 72 h / Heating 2: 59 percent / formic acid / 10 h / Heating 3: 25 percent / benzene / 48 h / Heating 4: 66.6 percent / 6N HCl / 48 h / Heating View Scheme
参考文献
Charles, Elisabeth S.; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 752 - 756
29906-47-6
→
反应条件
25057-77-6
1,2-二甲基哌嗪
反应条件
1: 70 percent / lithium aluminium hydride / tetrahydrofuran / 72 h / Heating 2: 67 percent / triethylamine / benzene / Heating 3: 70 percent / hydrogen / 10percent Pd-C / acetic acid / 12 h / 1838.8 Torr 4: 63 percent / triethylamine / acetone / Ambient temperature 5: 61 percent / dil. HCl / 24 h / Heating View Scheme
参考文献
Charles, Elisabeth S.; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 752 - 756
29906-47-6
→
反应条件
29906-54-5
N-1-苄基-2-甲基哌嗪
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 72 h; Heating;
参考文献
Charles, Elisabeth S.; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 752 - 756
29906-47-6
→
反应条件
114649-85-3
乙基2,4-二甲基-1-哌嗪羧酸酯
反应条件
1: 70 percent / lithium aluminium hydride / tetrahydrofuran / 72 h / Heating 2: 59 percent / formic acid / 10 h / Heating 3: 25 percent / benzene / 48 h / Heating View Scheme
参考文献
Charles, Elisabeth S.; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 752 - 756
29906-47-6
→
反应条件
114649-94-4
乙基3,4-二甲基-1-哌嗪羧酸酯
反应条件
1: 70 percent / lithium aluminium hydride / tetrahydrofuran / 72 h / Heating 2: 67 percent / triethylamine / benzene / Heating 3: 70 percent / hydrogen / 10percent Pd-C / acetic acid / 12 h / 1838.8 Torr 4: 63 percent / triethylamine / acetone / Ambient temperature View Scheme
参考文献
Charles, Elisabeth S.; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 752 - 756
29906-47-6
→
反应条件
114649-88-6
N,N,3,4-四甲基-1-哌嗪甲酰胺
反应条件
1: 70 percent / lithium aluminium hydride / tetrahydrofuran / 72 h / Heating 2: 60 percent / triethylamine / benzene / Heating 3: 68 percent / hydrogen / 10percent Pd-C / acetic acid / 1838.8 Torr 4: 68 percent / triethylamine / acetone / 48 h / Ambient temperature View Scheme
参考文献
Charles, Elisabeth S.; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 752 - 756
29906-47-6
→
反应条件
114649-92-2
N,N,3-三甲基哌嗪-1-甲酰胺
反应条件
1: 70 percent / lithium aluminium hydride / tetrahydrofuran / 72 h / Heating 2: 60 percent / triethylamine / benzene / Heating 3: 68 percent / hydrogen / 10percent Pd-C / acetic acid / 1838.8 Torr View Scheme
参考文献
Charles, Elisabeth S.; Sharma, Satyavan
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1987 , vol. 26, # 1-12 p. 752 - 756
