2,3,4-戊三酮肟 (6ci,7ci,8ci,9ci)合成路线 (共 37 条)
反应条件
sulfuric acid; sodium nitrite in water T=20°C; 2 h;
参考文献
Nikitina, Polina A.; Kuz'Mina, Ludmila G.; Perevalov, Valery P.; Tkach, Iosif I.
Tetrahedron, 2013 , vol. 69, # 15 p. 3249 - 3256
反应条件
tert.-butylnitrite; sulfuric acid in acetonitrile T=25°C; different AA, reagent and H2SO4 concentations; effect of added t-butyl alcohol or isopropyl alcohol; Rate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 1015 - 1020
反应条件
nitryl chloride in dichloromethane T=40°C; 2 h; 1) variation of molar ratio of NO2Cl/educt; Product distribution;
参考文献
Monatshefte fuer Chemie, , vol. 111, p. 771 - 774
参考文献
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, , vol. 155, p. 180
参考文献
Chemische Berichte, , vol. 45, p. 1340
反应条件
ethanol; nickel T=80°C; P=73550.8 Torr; Hydrogenation;
参考文献
Treibs et al.
Chemische Berichte, 1957 , vol. 90, p. 79,81
反应条件
amalgamated zinc; acetic acid Behandeln des Reaktionsprodukts mit PCl5 oder SOCl2;
参考文献
Treibs; Sutter
Chemische Berichte, 1951 , vol. 84, p. 96,99
参考文献
Padmavathy; Nagendrappa, Gopalpur; Geetha
Tetrahedron Letters, 2011 , vol. 52, # 4 p. 544 - 547
反应条件
triethylamine in acetonitrile 6 h; Heating; Mechanism;
参考文献
Veronese, A.C.; Cavicchioni, G.; Servadio, G.; Vecchiati, G.
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 1723 - 1725
反应条件
molecular sieve in acetone T=20°C; Condensation; Cyclization;
参考文献
Semichenko; Belyaev
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 9 p. 1385 - 1385