2,3,4-戊三酮肟 (6ci,7ci,8ci,9ci)合成路线 （共 37 条）
反应条件
molecular sieve Condensation; Cyclization;
参考文献
Semichenko; Belyaev
Russian Journal of Organic Chemistry, 1999 , vol. 35, # 9 p. 1385 - 1385
反应条件
2: 74 percent / dimethylsulfoxide / 3 h / 100 °C View Scheme
参考文献
Veronese, A.C.; Cavicchioni, G.; Servadio, G.; Vecchiati, G.
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 1723 - 1725
反应条件
sulfuric acid; zinc Diazotieren des entstehenden Reduktionsprodukts;
参考文献
Staudinger; Gaule
Chemische Berichte, 1916 , vol. 49, p. 1915
Full Text Show Details
Wolff
Justus Liebigs Annalen der Chemie, 1902 , vol. 325, p. 137
Justus Liebigs Annalen der Chemie, 1912 , vol. 394, p. 46 Anm. 2
反应条件
1: ethanol 2: 76 percent / LiAlH4 / diethyl ether / 3 h / 25 °C View Scheme
参考文献
Cuadrado, Purificacion; Gonzalez-Nogal, Ana M.; Martinez, Senen
Tetrahedron, 1997 , vol. 53, # 25 p. 8585 - 8598
反应条件
ethanol; nickel T=70 - 90°C; Hydrogenation;
参考文献
Kuester
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1922 , vol. 121, p. 146
参考文献
Veronese, A.C.; Cavicchioni, G.; Servadio, G.; Vecchiati, G.
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 1723 - 1725
反应条件
1: hydroxylamine hydrochloride, sodium acetate trihydrate / H2O / 17 h / 5 °C 2: 20 percent / cerium(IV) ammonium nitrate / acetic acid; H2O / 2 h / Ambient temperature View Scheme
参考文献
Fruttero, Roberta; Calvino, Rosella; Ferrarotti, Bruno; Gasco, Alberto; Aime, Silvio; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1987 , p. 523 - 530
反应条件
1: With hydrogenchloride; acetic acid T=0 - 5°C; 2: With acetic acid; zinc T=40 - 50°C; 5 h;
参考文献
Zhang, Caihong; Li, Lifeng; Wu, Hongjuan; Liu, Zhixun; Li, Junfen; Zhang, Guomei; Wen, Guangming; Shuang, Shaomin; Dong, Chuan; Choi, Martin M.F.
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2013 , vol. 102, p. 256 - 262
反应条件
1: natrium carbonate; hydrazine sulfate 2: concentrated nitric acid View Scheme
参考文献
Wolff
Justus Liebigs Annalen der Chemie, 1902 , vol. 325, p. 137
Justus Liebigs Annalen der Chemie, 1912 , vol. 394, p. 46 Anm. 2
反应条件
sodium ethanolate in dimethyl sulfoxide 1 h;
参考文献
Belyaev, E. Yu.; El'tsov, A. V.; Kochetkov, B. B.; Orlovskaya, N. F.; Tovbis, M. S.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1299 - 1304
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 7 p. 1489 - 1495
