1: pentadiene-1,4 With n-butyllithium; potassium tert-butylate in hexane; Petroleum ether T=0°C; 0.333333 h; 2: carbon dioxide in tetrahydrofuran; hexane T=-75°C; Title compound not separated from byproducts;
phenyl-sodium; benzene und Umsetzung des Reaktionsprodukts mit festem CO2 bei 3grad;
参考文献
Paul; Tchelitcheff
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1947 , vol. 224, p. 1118
Bulletin de la Societe Chimique de France, 1948 , p. 111,113
dicyclohexyl-carbodiimide in pyridine; dichloromethane
参考文献
Lawson, Kevin R.; McDonald, Brian P.; Mills, Owen S.; Steele, Robert W.; Sutherland, James K.; et.al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 663 - 674