1-(2-羟基-5-甲基)-3-苯基-1,3-丙烷二酮合成路线 （共 20 条）
反应条件
potassium hydroxide in methanol T=50°C; 0.25 h;
参考文献
Mumtazuddin
Journal of the Indian Chemical Society, 2006 , vol. 83, # 8 p. 835 - 837
反应条件
1: 91 percent / pyridine / 0.17 h / 70 °C 2: 54 percent / t-BuOK / tetrahydrofuran / 0.17 h / 20 °C View Scheme
参考文献
Chemistry Letters, , vol. 36, # 4 p. 522 - 523
反应条件
barium dihydroxide in dimethyl sulfoxide 0.00694444 h; microwave irradiation;
参考文献
Lamba; Kumar, Suresh; Makrandi
Journal of Chemical Research, 2006 , # 2 p. 133 - 134
反应条件
1: pyridine 2: 85percent KOH / pyridine / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 56, # 26 p. 7292 - 7297
反应条件
1: 68 percent / 4-dimethylaminopyridine, N,N'-dicyclohexylcarbodiimide / CHCl3 / 0.25 h / Ambient temperature 2: 90 percent / 20percent H2SO4, SiO2 / CHCl3 / 6 h 3: 17 percent / hexane / 6 h / Ambient temperature; Irradiation View Scheme
参考文献
Heterocycles, , vol. 24, # 9 p. 2511 - 2517
反应条件
1: 10 percent NaOH / 1 h / Heating 2: 68 percent / 4-dimethylaminopyridine, N,N'-dicyclohexylcarbodiimide / CHCl3 / 0.25 h / Ambient temperature 3: 90 percent / 20percent H2SO4, SiO2 / CHCl3 / 6 h 4: 17 percent / hexane / 6 h / Ambient temperature; Irradiation View Scheme
参考文献
Heterocycles, , vol. 24, # 9 p. 2511 - 2517
反应条件
1: p-toluenesulphonic acid / benzene / Heating 2: 10 percent NaOH / 1 h / Heating 3: 68 percent / 4-dimethylaminopyridine, N,N'-dicyclohexylcarbodiimide / CHCl3 / 0.25 h / Ambient temperature 4: 90 percent / 20percent H2SO4, SiO2 / CHCl3 / 6 h 5: 17 percent / hexane / 6 h / Ambient temperature; Irradiation View Scheme
参考文献
Heterocycles, , vol. 24, # 9 p. 2511 - 2517
反应条件
1: 68 percent / 4-dimethylaminopyridine, N,N'-dicyclohexylcarbodiimide / CHCl3 / 0.25 h / Ambient temperature 2: 90 percent / 20percent H2SO4, SiO2 / CHCl3 / 6 h 3: 17 percent / hexane / 6 h / Ambient temperature; Irradiation View Scheme
参考文献
Heterocycles, , vol. 24, # 9 p. 2511 - 2517
反应条件
1: 90 percent / 20percent H2SO4, SiO2 / CHCl3 / 6 h 2: 17 percent / hexane / 6 h / Ambient temperature; Irradiation View Scheme
参考文献
Heterocycles, , vol. 24, # 9 p. 2511 - 2517
反应条件
1: AlCl3, aluminium chloride / 2 h / 120 - 180 °C 2: potassium carbonate / acetone / 12 h / |Reflux View Scheme
参考文献
Medicinal Chemistry Research, , vol. 21, # 8 p. 1833 - 1849,17
