2-(2-丙炔氧基)苯甲醛合成路线 (共 17 条)
反应条件
tetra-n-butylammonium tetrafluoroborate; [Ni(2,2'-bipyridine)3(2+)][BF4(1-)]2 in N,N-dimethyl-formamide electrochem. reaction; magnesium rod anode, nickel foam grid cathode;
参考文献
Tetrahedron Letters, , vol. 40, # 15 p. 2951 - 2954
反应条件
pyridine; hydroxylamine hydrochloride in ethanol Reflux;
参考文献
Roy, Brindaban; De, Rajendra Narayan
Monatshefte fur Chemie, 2010 , vol. 141, # 7 p. 763 - 771
反应条件
1: With C23H31AuN(1+)*F6Sb(1-); benzyl alcohol in dichloromethane
T=20°C; 1 h; in air;
2: With toluene-4-sulfonic acid in dichloromethane
T=40°C; 6 h; in air;
参考文献
Sze, Ella Min Ling; Rao, Weidong; Koh, Ming Joo; Chan, Philip Wai Hong
Chemistry - A European Journal, 2011 , vol. 17, # 5 p. 1437 - 1441
反应条件
acetic acid; tris(acetonitrile)(η5-2,4-cyclopentadien-1-yl)ruthenium(1+) hexafluorophosphate(1-)
T=90°C; 24 h;
参考文献
Varela, Jesus A.; Gonzalez-Rodriguez, Carlos; Rubin, Silvia G.; Castedo, Luis; Saa, Carlos
Journal of the American Chemical Society, 2006 , vol. 128, # 30 p. 9576 - 9577
反应条件
copper(l) iodide; lanthanum trifluoromethanesulphonate in acetonitrile
3 h; Reflux;
参考文献
Ramesh, Subburethinam; Gaddam, Vikram; Nagarajan, Rajagopal
Synlett, 2010 , # 5 p. 757 - 760
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in tetrahydrofuran
Inert atmosphere;
参考文献
Xia, Xiao-Feng; Song, Xian-Rong; Liu, Xue-Yuan; Liang, Yong-Min
Chemistry - An Asian Journal, 2012 , vol. 7, # 7 p. 1538 - 1541
反应条件
acetic acid in ethanol
0.25 h; Heating;
参考文献
Mignot; Miocque; Binet; et al.
European Journal of Medicinal Chemistry, 1980 , vol. 15, # 1 p. 33 - 40