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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3004-58-8
合成路线
（共 20 条）
685-91-6
N,N-二乙基乙酰胺
+
108-90-7
氯苯
→
反应条件
3004-58-8
反应条件
C40H45N2O3PPdS; sodium t-butanolate T=110°C; Inert atmosphere; chemoselective reaction;
参考文献
Zheng, Bing; Jia, Tiezheng; Walsh, Patrick J.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 1 p. 165 - 178
685-91-6
N,N-二乙基乙酰胺
+
108-86-1
溴代苯
→
反应条件
3004-58-8
反应条件
N-(dicyclohexylphosphino)-2-(2'-tolyl)-1H-indole; palladium diacetate; sodium hexamethyldisilazane in toluene T=110°C; Inert atmosphereSealed tubeMicrowave irradiation; chemoselective reaction;
参考文献
Zheng, Bing; Jia, Tiezheng; Walsh, Patrick J.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 1 p. 165 - 178
108-86-1
溴代苯
+
2431-96-1
N,N-二乙基苯乙酰胺
→
反应条件
3004-58-8
反应条件
N-(dicyclohexylphosphino)-2-(2'-tolyl)-1H-indole; palladium diacetate; sodium t-butanolate in toluene T=110°C; Inert atmosphereSealed tubeMicrowave irradiation;
参考文献
Zheng, Bing; Jia, Tiezheng; Walsh, Patrick J.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 1 p. 165 - 178
685-91-6
N,N-二乙基乙酰胺
+
108-90-7
氯苯
→
反应条件
2431-96-1
N,N-二乙基苯乙酰胺
+
3004-58-8
反应条件
N-(dicyclohexylphosphino)-2-(2'-tolyl)-1H-indole; C24H16Cl2N2Pd2; lithium tert-butylate T=110°C; Inert atmosphere; chemoselective reaction;
参考文献
Zheng, Bing; Jia, Tiezheng; Walsh, Patrick J.
Organic Letters, 2013 , vol. 15, # 16 p. 4190 - 4193
2431-96-1
N,N-二乙基苯乙酰胺
+
108-90-7
氯苯
→
反应条件
3004-58-8
反应条件
C27H34NP*C13H13NO3PdS; sodium t-butanolate T=110°C; Inert atmosphereSealed tubeMicrowave irradiation; Reagent/catalyst;
参考文献
Zheng, Bing; Jia, Tiezheng; Walsh, Patrick J.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 1 p. 165 - 178
1871-76-7
二苯基乙酰氯
+
109-89-7
二乙胺
→
反应条件
3004-58-8
反应条件
Petroleum ether
参考文献
Laval, Stephane; Dayoub, Wissam; Favre-Reguillon, Alain; Demonchaux, Patrice; Mignani, Gerard; Lemaire, Marc
Tetrahedron Letters, 2010 , vol. 51, # 16 p. 2092 - 2094
81838-75-7
→
反应条件
3004-58-8
反应条件
sulfuric acid; dodecanesulphonic acid sodium salt; sodium nitrite
参考文献
Eckstein, Z.; Jelenski, P.; Kowal, J.; Rusek, D.
Synthetic Communications, 1982 , vol. 12, # 3 p. 201 - 208
685-91-6
N,N-二乙基乙酰胺
+
108-86-1
溴代苯
→
反应条件
2431-96-1
N,N-二乙基苯乙酰胺
+
3004-58-8
反应条件
N-(dicyclohexylphosphino)-2-(2'-tolyl)-1H-indole; palladium diacetate; lithium hexamethyldisilazane in toluene T=110°C; Inert atmosphereSealed tubeMicrowave irradiation; chemoselective reaction;
参考文献
Zheng, Bing; Jia, Tiezheng; Walsh, Patrick J.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 1 p. 165 - 178
685-91-6
N,N-二乙基乙酰胺
→
反应条件
3004-58-8
反应条件
1: palladium diacetate; N-(dicyclohexylphosphino)-2-(2'-tolyl)-1H-indole; lithium tert-butylate / toluene / 12 h / 110 °C / |Inert atmosphere; |Sealed tube; |Microwave irradiation 2: palladium diacetate; N-(dicyclohexylphosphino)-2-(2'-tolyl)-1H-indole; sodium t-butanolate / toluene / 110 °C / |Inert atmosphere; |Sealed tube; |Microwave irradiation View Scheme
参考文献
Zheng, Bing; Jia, Tiezheng; Walsh, Patrick J.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 1 p. 165 - 178
108-86-1
溴代苯
→
反应条件
3004-58-8
反应条件
1: palladium diacetate; N-(dicyclohexylphosphino)-2-(2'-tolyl)-1H-indole; lithium tert-butylate / toluene / 12 h / 110 °C / |Inert atmosphere; |Sealed tube; |Microwave irradiation 2: palladium diacetate; N-(dicyclohexylphosphino)-2-(2'-tolyl)-1H-indole; sodium t-butanolate / toluene / 110 °C / |Inert atmosphere; |Sealed tube; |Microwave irradiation View Scheme
参考文献
Zheng, Bing; Jia, Tiezheng; Walsh, Patrick J.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 1 p. 165 - 178
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