2,3-二溴-N-甲基马来酰亚胺合成路线 （共 24 条）
反应条件
in acetone
Irradiation;
参考文献
Szilagyi, Geza; Wamhoff, Heinrich
Angewandte Chemie, 1983 , vol. 95, # 2 p. 156 - 157
反应条件
1: 90 percent / Ce / 0 °C
2: 75 percent / MCPBA / 56 °C
3: Zn/Ag
4: 71 percent
5: 88 percent / 165 °C
6: tetrahydrofuran / 0 °C / Irradiation
View Scheme
参考文献
Pitt, Ian G.; Russell, Richard, A.; Warrener, Ronald N.
Journal of the American Chemical Society, 1985 , vol. 107, # 24 p. 7176 - 7178
反应条件
triethylamine in N,N-dimethyl-formamide
T=20°C;
参考文献
Lakatosh, Sergey A.; Luzikov, Yuri N.; Preobrazhenskaya, Maria N.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 5 p. 826 - 833
反应条件
1: indole With lithium hexamethyldisilazane in tetrahydrofuran; hexane
T=-15°C; 1.16667 h;
2: 3,4-dibromo-N-methylmaleimide in tetrahydrofuran; hexane
T=-15 - 20°C; 0.583333 h;
3: With hydrogenchloride in tetrahydrofuran; hexane; water
pH=7;
参考文献
Coudert, Gerard; Ayerbe, Nathalie; Lepiere, Franck; Routier, Sylvain; Caignard, Daniel-Henri; Renard, Pierre; Hickman, John; Pierre, Alain; Leonce, Stephane
Patent: US2006/40930 A1, 2006 ;
Location in patent: Page/Page column 11 ;
