反应条件
n-BuLi in diethyl ether
under N2 atm. soln. CF3CH2CF2H in Et2O at -10°C was treated with n-BuLi, after 10 min Ph3GeBr in Et2O was added and stirred at 0°Covernight and warmed to room temp.; hexane was added, soln. was filtered, concd. in vacuo, and chromed. on silica; elem. anal.;
参考文献
Brisdon, Alan K.; Crossley, Ian R.; Pritchard, Robin G.; Sadiq, Ghazala; Warren, John E.
Organometallics, 2003 , vol. 22, # 26 p. 5534 - 5542
