二(亚磷酸三苯酯)二氯化铂(II)合成路线 （共 5 条）
反应条件
in benzene (N2), soln. of Pt complex in benzene treated with 2 equiv. of phosphane,stirred at room temp. for 1 h; filtered, washed (benzene);
参考文献
Kajiyama, Kazumasa; Sato, Issei; Yamashita, Satoru; Miyamoto, Takeshi K.
European Journal of Inorganic Chemistry, 2009 , # 36 p. 5516 - 5521
反应条件
in dichloromethane stirring (10 min); pptn. with pentane, filtration, washing (pentane), drying (vac.);
参考文献
Albinati; Affolter; Pregosin
Organometallics, 1990 , vol. 9, # 2 p. 379 - 387
反应条件
in melt addn. of PtCl2 to melt of ligand (stirring, 30 min); cooling to room temp., dissolution in CHCl3, filtration (Celite), pptn. on Et2O addn., sepn. (centrifugation);
参考文献
Bruce, Duncan W.; Donnio, Bertrand; Maggs, Andrew A.; Marsden, Julian R.
Inorganica Chimica Acta, 1991 , vol. 188, p. 41 - 44
反应条件
in tetrahydrofuran byproducts: NaCl; inert atmosphere; stirring (-20°C, 6 h); evapn. to dryness (-10°C), dissoln. in toluene, filtration, chromy. (Florisil, hexane, then hexane/Et2O);
参考文献
New Journal of Chemistry, , vol. 14, p. 569 - 582
反应条件
silver carbonate
under N2;
参考文献
Almeida, Joaquim F.; Azizian, Hormoz; Eaborn, Colin; Pidcock, Alan
Journal of Organometallic Chemistry, 1981 , vol. 210, # 1 p. 121 - 134
