3-氯-苯甲酸 1,1'-酸酐合成路线 （共 11 条）
参考文献
Kaminski, Zbigniew J.; Kolesinska, Beata; Malgorzata, Marcinkowska
Synthetic Communications, 2004 , vol. 34, # 18 p. 3349 - 3358
反应条件
palladium diacetate; ethylene dibromide T=100°C; P=11400 Torr; 20 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Fujiwara, Yuzo; Kawata, Itaru; Kawauchi, Tomio; Taniguchi, Hiroshi
Journal of the Chemical Society, Chemical Communications, 1982 , # 2 p. 132 - 133
反应条件
C22H29N3O3; triethylamine; C16H23P*BF4(1-)*H(1+) in toluene T=-40°C; 3 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Duffey, Trisha A.; MacKay, James A.; Vedejs, Edwin
Journal of Organic Chemistry, 2010 , vol. 75, # 14 p. 4674 - 4685
参考文献
Bayer Aktiengesellschaft
Patent: US4238412 A1, 1980 ;
反应条件
sodium carbonate; palladium dichloride in water; acetone T=20°C; Suzuki type reaction; 1.5 h; Inert atmosphere;
参考文献
Xin, Bing-Wei
Synthetic Communications, 2008 , vol. 38, # 16 p. 2826 - 2837
反应条件
PEG200; sodium carbonate; palladium diacetate T=60°C; Suzuki reaction; 2 h;
参考文献
Xin, Bingwei; Zhang, Yuhong; Cheng, Kai
Journal of Organic Chemistry, 2006 , vol. 71, # 15 p. 5725 - 5731
反应条件
Wilkinson's catalyst T=240°C;
参考文献
Blum,J. et al.
Journal of Organic Chemistry, 1970 , vol. 35, p. 3233 - 3237
反应条件
triethylamine; C16H23P*BF4(1-)*H(1+) in toluene T=-40°C; 6 h; Inert atmosphereResolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Duffey, Trisha A.; MacKay, James A.; Vedejs, Edwin
Journal of Organic Chemistry, 2010 , vol. 75, # 14 p. 4674 - 4685
反应条件
C22H29N3O3; triethylamine; C16H23P*BF4(1-)*H(1+) in toluene T=-40°C; 3 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Duffey, Trisha A.; MacKay, James A.; Vedejs, Edwin
Journal of Organic Chemistry, 2010 , vol. 75, # 14 p. 4674 - 4685
反应条件
Wilkinson's catalyst
T=240°C;
参考文献
Blum,J. et al.
Journal of Organic Chemistry, 1970 , vol. 35, p. 3233 - 3237
