7-甲基-2-苯基-咪唑并[1,2-a]吡啶-3-甲醛合成路线 （共 4 条）
反应条件
[copperl(II)(1,1,1,5,5,5-hexafluoroacetylacetonate)2] monohydrate; oxygen in N,N-dimethyl-formamide T=105°C; 10 h;
参考文献
Wang, Honggen; Wang, Yong; Liang, Dongdong; Liu, Lanying; Zhang, Jiancun; Zhu, Qiang
Angewandte Chemie - International Edition, 2011 , vol. 50, # 25 p. 5678 - 5681
反应条件
1: toluene-4-sulfonic acid / tetrahydrofuran / 18 h / Molecular sieve; Inert atmosphere; Reflux 2: tetrahydrofuran / -78 - 20 °C / Molecular sieve; Inert atmosphere 3: [copperl(II)(1,1,1,5,5,5-hexafluoroacetylacetonate)2] monohydrate; oxygen / N,N-dimethyl-formamide / 10 h / 105 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 25 p. 5678 - 5681
反应条件
1: toluene-4-sulfonic acid / tetrahydrofuran / 18 h / Molecular sieve; Inert atmosphere; Reflux 2: tetrahydrofuran / -78 - 20 °C / Molecular sieve; Inert atmosphere 3: [copperl(II)(1,1,1,5,5,5-hexafluoroacetylacetonate)2] monohydrate; oxygen / N,N-dimethyl-formamide / 10 h / 105 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 25 p. 5678 - 5681
反应条件
1: tetrahydrofuran / -78 - 20 °C / Molecular sieve; Inert atmosphere 2: [copperl(II)(1,1,1,5,5,5-hexafluoroacetylacetonate)2] monohydrate; oxygen / N,N-dimethyl-formamide / 10 h / 105 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 25 p. 5678 - 5681
