1,1-二甲氧基-3-苯基丙烷合成路线 （共 26 条）
反应条件
1: 1,1-dimethoxy-3-phenylpropane With bromine in dichloromethane T=25 - 30°C; Bromination; 2: methanol alcoholysis; 0.05 h; Further stages.;
参考文献
Journal of Organic Chemistry, , vol. 65, # 7 p. 2151 - 2162
反应条件
1: 90 percent / trityl perchlorate / CH2Cl2 / 0.08 h / 0 °C 2: 94 percent / methanol; various solvent(s) / 60 °C View Scheme
参考文献
Mukaiyama, Teruaki; Kato, Jun-ichi; Miyoshi, Norikazu; Iwasawa, Nobuharu
Chemistry Letters, 1985 , p. 1255 - 1258
反应条件
tin(ll) chloride; C60-soot in dichloromethane 0.75 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 58, # 15 p. 4142 - 4143
反应条件
1.1: Br2 / CH2Cl2 / 25 - 30 °C 1.2: 89 percent / 0.05 h 2.1: K2CO3; N2H4*H2O; Ph2Se2 / dimethylsulfoxide / 7 h / 70 °C 2.2: Et3N; 30percent H2O2 / tetrahydrofuran / 5 h / 20 °C 2.3: 59 percent / oxalic acid / acetone; H2O / 1 h / 20 °C View Scheme
参考文献
Vasil'ev, Andrei; Engman, Lars
Journal of Organic Chemistry, 2000 , vol. 65, # 7 p. 2151 - 2162
反应条件
indium trifluoromethanesulfonate in dichloromethane
T=20°C; 0.0833333 h;
参考文献
Smith, Brendan M.; Graham, Andrew E.
Tetrahedron Letters, 2006 , vol. 47, # 52 p. 9317 - 9319
反应条件
[[RhCl(COD)]2(1,4-bis(diphenylphosphinoxy)benzene)]; hydrogen
T=80°C; P=22502.3 Torr; 8 h; AutoclaveInert atmosphere; regioselective reaction;
参考文献
Khan, Shoeb R.; Bhanage, Bhalchandra M.
Tetrahedron Letters, 2013 , vol. 54, # 45 p. 5998 - 6001
反应条件
hydrogen; palladium on activated charcoal
T=20°C; 18 h;
参考文献
Yang, Bai-Ling; Tian, Shi-Kai
European Journal of Organic Chemistry, 2007 , # 28 p. 4646 - 4650
反应条件
hydroxylamine hydrochloride; sodium hydroxide
T=20°C; 18 h; chemoselective reaction;
参考文献
Mickelsen, Ky J.; Tajc, Chelsea M.; Greenwood, Kevin R.; Browder, Cindy C.
Synthetic Communications, 2012 , vol. 42, # 2 p. 186 - 194
反应条件
ammonia; titanium tetrachloride in dichloromethane
T=0°C;
参考文献
Clerici, Angelo; Pastori, Nadia; Porta, Ombretta
Tetrahedron, 1998 , vol. 54, # 51 p. 15679 - 15690
反应条件
platinum (II) chloride
T=70°C; 20 h; Inert atmosphereneat (no solvent);
参考文献
Munoz, Maria Paz; De La Torre, Maria C.; Sierra, Miguel A.
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 13 p. 2189 - 2194
