1,1-二甲氧基-3-苯基丙烷合成路线 （共 26 条）
反应条件
1: 83 percent / HClO4-SiO2 / 0.17 h / 25 - 30 °C
2: 86 percent / HClO4-SiO2 / H2O; ethanol / 0.25 h / 25 - 30 °C
3: 85 percent / HClO4-SiO2 / 0.03 h / 25 - 30 °C
View Scheme
参考文献
Kumar, Raj; Kumar, Dinesh; Chakraborti, Asit K.
Synthesis, 2007 , # 2 p. 299 - 303
反应条件
1: 86 percent / HClO4-SiO2 / H2O; ethanol / 0.25 h / 25 - 30 °C
2: 85 percent / HClO4-SiO2 / 0.03 h / 25 - 30 °C
View Scheme
参考文献
Kumar, Raj; Kumar, Dinesh; Chakraborti, Asit K.
Synthesis, 2007 , # 2 p. 299 - 303
反应条件
bis(dibenzylideneacetone)-palladium(0)
T=50°C; Heck arylation; 2 h; Title compound not separated from byproducts;
参考文献
Masllorens, Judit; Bouquillon, Sandrine; Roglans, Anna; Henin, Francoise; Muzart, Jacques
Journal of Organometallic Chemistry, 2005 , vol. 690, # 16 p. 3822 - 3826
反应条件
methanol; hydrogen; palladium
参考文献
Straus; Berkow
Justus Liebigs Annalen der Chemie, 1913 , vol. 401, p. 143
反应条件
1: (i) LDA, tetramethylethylendiamine, THF, (ii) /BRN= 2040359/
2: N-chloro-succinimide, Et3N
View Scheme
参考文献
Mendoza,A.; Matteson,D.S.
Journal of Organometallic Chemistry, 1978 , vol. 156, p. 149 - 157
反应条件
N-chloro-succinimide; triethylamine
参考文献
Mendoza,A.; Matteson,D.S.
Journal of Organometallic Chemistry, 1978 , vol. 156, p. 149 - 157
反应条件
hydrogenchloride; palladium on activated charcoal
Hydrogenation;
参考文献
Gen. Aniline and Film Corp.
Patent: US2516679 , 1948 ;
反应条件
2: sodium; alcohol / Verseifen des entstandenen Acetals mit Schwefelsaeure
View Scheme
参考文献
Fischer,E.; Hoffa
Chemische Berichte, 1898 , vol. 31, p. 1990
反应条件
ammonium cerium(IV) nitrate
10 h; Ambient temperature;
参考文献
Hanessian, Stephen; Ninkovic, Sacha
Canadian Journal of Chemistry, 1996 , vol. 74, # 10 p. 1880 - 1888
参考文献
Fischer,E.; Hoffa
Chemische Berichte, 1898 , vol. 31, p. 1990
